C₂₉H₄₅N₃O₄S

Base Information

• Chemical Name: C₂₉H₄₅N₃O₄S
• CAS No.: 1241383-31-2
• Molecular Formula: C₂₉H₄₅N₃O₄S
• Molecular Weight: 531.76
• Mol file: 1241383-31-2.mol

Synonyms:C₂₉H₄₅N₃O₄S

Chemical Property of C₂₉H₄₅N₃O₄S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₉H₄₅N₃O₄S

There total 5 articles about C₂₉H₄₅N₃O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-mesitylenesulphonyl chloride (773-64-8) + C20H35N3O2 (1241383-28-7) → C29H45N3O4S (1241383-31-2)

Guidance literature:

With sodium hydroxide; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1007/s11095-010-0197-4

Reference yield:

N-ethylbenzylamine (14321-27-8) → C29H45N3O4S (1241383-31-2)

Guidance literature:

Multi-step reaction with 6 steps

1: monohydrate copper acetate / water; acetonitrile / 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere; Reflux

3: triethylamine / dichloromethane / 1 h / -10 °C / Inert atmosphere

4: dichloromethane / 24 h / 20 °C / Inert atmosphere

5: dichloromethane / 20 h / Inert atmosphere; Reflux

6: sodium hydroxide / dichloromethane / 24 h / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; monohydrate copper acetate; triethylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; acetonitrile; 1: Michael addition;

DOI:10.1007/s11095-010-0197-4

Reference yield:

3-(benzylethylamino)propanol (91553-67-2) → C29H45N3O4S (1241383-31-2)

Guidance literature:

Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 1 h / -10 °C / Inert atmosphere

2: dichloromethane / 24 h / 20 °C / Inert atmosphere

3: dichloromethane / 20 h / Inert atmosphere; Reflux

4: sodium hydroxide / dichloromethane / 24 h / 20 °C / Inert atmosphere

With triethylamine; sodium hydroxide; In dichloromethane;

DOI:10.1007/s11095-010-0197-4

upstream raw materials:

2-mesitylenesulphonyl chloride

C₂₀H₃₅N₃O₂

ethyl 3-(benzyl(ethyl)amino)propanoate

C₁₃H₂₁NO₃S

Downstream raw materials:

C₂₃H₄₁N₃O₄S

C₂₂H₃₉N₃O₄S

C₃₁H₄₉N₃O₆S₂

C₃₅H₆₂N₄O₆