[6-(18)O]β-hydroxyhyoscyamine

Base Information

Chemical Name:[6-(18)O]β-hydroxyhyoscyamine
CAS No.:109621-22-9
Molecular Formula:C₁₇H₂₃NO₄
Molecular Weight:307.375
Hs Code.:

Synonyms:[6-(18)O]β-hydroxyhyoscyamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [6-(18)O]β-hydroxyhyoscyamine

Chemical Property:

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Technology Process of [6-(18)O]β-hydroxyhyoscyamine

There total 4 articles about [6-(18)O]β-hydroxyhyoscyamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 101-31-5
Hyoscyamine

: 109621-22-9
[6-(18)O]β-hydroxyhyoscyamine

: C₁₇H₂₃NO₃⁽¹⁸⁾O

: 17659-49-3,32671-33-3,76831-52-2,85760-60-7,126371-43-5,134355-54-7,138876-55-8,55869-99-3
(-)-Anisodamine

: 126371-43-5
7b-Hydroxyhyoscyamine

Guidance literature:: With diammonium iron(II) sulfate hexahydrate; Hyoscyamus niger recombinant hyoscyamine 6β-hydroxylase; water; oxygen; α-ketoglutarate; In glycerol; at 20 ℃; for 0.166667h; pH=7.5; Mechanism; Enzymatic reaction;
DOI:10.1021/jacs.9b06689

Reference yield:

: [6β-²H]hyoscyamine

: 109621-22-9
[6-(18)O]β-hydroxyhyoscyamine

: C₁₇H₂₂⁽²⁾HNO₄

: C₁₇H₂₂⁽²⁾HNO₃⁽¹⁸⁾O

: 17659-49-3,32671-33-3,76831-52-2,85760-60-7,126371-43-5,134355-54-7,138876-55-8,55869-99-3
(-)-Anisodamine

Guidance literature:: With diammonium iron(II) sulfate hexahydrate; Hyoscyamus niger recombinant hyoscyamine 6β-hydroxylase; water; α-ketoglutarate; oxygen-18; In glycerol; at 20 ℃; for 0.166667h; pH=7.5; Mechanism; Enzymatic reaction;
DOI:10.1021/jacs.9b06689

Reference yield:

: 6415-90-3,50700-39-5,306-03-6,4607-53-8
(-)-hyoscyamine hydrobromide

: 109621-22-9
[6-(18)O]β-hydroxyhyoscyamine

Guidance literature:: With α-ketoglutaric acid; Atropa belladonna C-terminally hexahistidine-tagged hyoscyamine 6β-hydroxylase; iron(II) sulfate; sodium L-ascorbate; catalase; oxygen-18; for 2h; pH=7.6; aq. buffer; Enzymatic reaction;
DOI:10.1016/j.bmc.2012.05.042