(2E,2'E)-dimethyl 3,3'-(2,2'-(3,3'-sulfonylbis(prop-1-yne-3,1-diyl))bis(2,1-phenylene))diacrylate

Base Information

Chemical Name:(2E,2'E)-dimethyl 3,3'-(2,2'-(3,3'-sulfonylbis(prop-1-yne-3,1-diyl))bis(2,1-phenylene))diacrylate
CAS No.:1393727-06-4
Molecular Formula:C₂₆H₂₂O₆S
Molecular Weight:462.523
Hs Code.:

Synonyms:(2E,2'E)-dimethyl 3,3'-(2,2'-(3,3'-sulfonylbis(prop-1-yne-3,1-diyl))bis(2,1-phenylene))diacrylate

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Chemical Property of (2E,2'E)-dimethyl 3,3'-(2,2'-(3,3'-sulfonylbis(prop-1-yne-3,1-diyl))bis(2,1-phenylene))diacrylate

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Technology Process of (2E,2'E)-dimethyl 3,3'-(2,2'-(3,3'-sulfonylbis(prop-1-yne-3,1-diyl))bis(2,1-phenylene))diacrylate

There total 7 articles about (2E,2'E)-dimethyl 3,3'-(2,2'-(3,3'-sulfonylbis(prop-1-yne-3,1-diyl))bis(2,1-phenylene))diacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1393727-03-1
(2E,2'E)-dimethyl 3,3'-(2,2'-(3,3'-thiobis(prop-1-yne-3,1-diyl))bis(2,1-phenylene))diacrylate

: 1393727-06-4
(2E,2'E)-dimethyl 3,3'-(2,2'-(3,3'-sulfonylbis(prop-1-yne-3,1-diyl))bis(2,1-phenylene))diacrylate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1016/j.tet.2012.06.001

Reference yield:

: 1393726-85-6
C₁₈H₂₀O₄

: 1393727-06-4
(2E,2'E)-dimethyl 3,3'-(2,2'-(3,3'-sulfonylbis(prop-1-yne-3,1-diyl))bis(2,1-phenylene))diacrylate

Guidance literature:: Multi-step reaction with 5 steps

1: pyridinium p-toluenesulfonate / ethanol / 6 h / 20 °C

2: triethylamine / dichloromethane / 0.17 h / 0 °C

3: lithium bromide / tetrahydrofuran / 2 h / 20 °C

4: sodium sulfide / methanol / 0.25 h / 20 °C

5: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 0 °C

With sodium sulfide; pyridinium p-toluenesulfonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; lithium bromide; In tetrahydrofuran; methanol; ethanol; dichloromethane;
DOI:10.1016/j.tet.2012.06.001

Reference yield:

: 1393726-97-0
C₁₃H₁₁BrO₂

: 1393727-06-4
(2E,2'E)-dimethyl 3,3'-(2,2'-(3,3'-sulfonylbis(prop-1-yne-3,1-diyl))bis(2,1-phenylene))diacrylate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium sulfide / methanol / 0.25 h / 20 °C

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 0 °C

With sodium sulfide; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane;
DOI:10.1016/j.tet.2012.06.001