sodium [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-D-glycero-α-D-galacto-2-nonulopyranosid]onate

Base Information

• Chemical Name: sodium [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-D-glycero-α-D-galacto-2-nonulopyranosid]onate
• CAS No.: 1241906-48-8
• Molecular Formula: C₂₈H₃₀ClF₂N₂O₉*Na
• Molecular Weight: 634.994

Synonyms:sodium [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-D-glycero-α-D-galacto-2-nonulopyranosid]onate

Chemical Property of sodium [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-D-glycero-α-D-galacto-2-nonulopyranosid]onate

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Technology Process of sodium [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-D-glycero-α-D-galacto-2-nonulopyranosid]onate

There total 1 articles about sodium [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-D-glycero-α-D-galacto-2-nonulopyranosid]onate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

methyl [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-D-glycero-α-D-galacto-2-nonulopyranosid]onate (1241906-47-7) → sodium [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-D-glycero-α-D-galacto-2-nonulopyranosid]onate (1241906-48-8)

Guidance literature:

With sodium hydroxide; In methanol; water; for 2h;

DOI:10.1016/j.carres.2010.03.010

Reference yield: 80.0%

sodium [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-D-glycero-α-D-galacto-2-nonulopyranosid]onate (1241906-48-8) + acetic anhydride (108-24-7) → sodium [(2,3-difluorobenzyl) 5-acetamido-4-O-acetyl-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-D-glycero-α-D-galacto-2-nonulopyranosid]onate (1241906-52-4)

Guidance literature:

With dmap; In pyridine; at 0 - 20 ℃;

DOI:10.1016/j.carres.2010.03.010

Reference yield: 37.0%

2-(thiophen-2-yl)ethyl isocynate (58749-51-2) + sodium [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-D-glycero-α-D-galacto-2-nonulopyranosid]onate (1241906-48-8) → sodium [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-4-O-(2-(2-thienyl)ethylcarbamoyl)-D-glycero-α-D-galacto-2-nonulopyranosid]onate (1241906-58-0)

Guidance literature:

With dmap; In pyridine; at 45 ℃; for 24h;

DOI:10.1016/j.carres.2010.03.010

upstream raw materials:

methyl [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-D-glycero-α-D-galacto-2-nonulopyranosid]onate

Downstream raw materials:

sodium [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-4-O-((2-methylfuran-3-yl)carbamoyl)-D-glycero-α-D-galacto-2-nonulopyranosid]onate

sodium [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-4-O-(2-(2-thienyl)ethylcarbamoyl)-D-glycero-α-D-galacto-2-nonulopyranosid]onate

sodium [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-4-O-(2-phenylethylcarbamoyl)-D-glycero-α-D-galacto-2-nonulopyranosid]onate

sodium [(2,3-difluorobenzyl) 5-acetamido-4-O-acetyl-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-D-glycero-α-D-galacto-2-nonulopyranosid]onate

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