(1R,3R,6R,10R)-8-benzyloxycarbonyl-3-phenyl-8-aza-2,4-dioxabicyclo[4.4.0]decan-10-ol

Base Information

Chemical Name:(1R,3R,6R,10R)-8-benzyloxycarbonyl-3-phenyl-8-aza-2,4-dioxabicyclo[4.4.0]decan-10-ol
CAS No.:727989-21-1
Molecular Formula:C₂₁H₂₃NO₅
Molecular Weight:369.417
Hs Code.:

Synonyms:(1R,3R,6R,10R)-8-benzyloxycarbonyl-3-phenyl-8-aza-2,4-dioxabicyclo[4.4.0]decan-10-ol

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Chemical Property of (1R,3R,6R,10R)-8-benzyloxycarbonyl-3-phenyl-8-aza-2,4-dioxabicyclo[4.4.0]decan-10-ol

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Technology Process of (1R,3R,6R,10R)-8-benzyloxycarbonyl-3-phenyl-8-aza-2,4-dioxabicyclo[4.4.0]decan-10-ol

There total 1 articles about (1R,3R,6R,10R)-8-benzyloxycarbonyl-3-phenyl-8-aza-2,4-dioxabicyclo[4.4.0]decan-10-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 774-48-1
(diethoxymethyl)benzene

: 568586-63-0
(3R,4R,5R)-N-benzyloxycarbonyl-3,4-dihydroxy-5-(hydroxymethyl)piperidine

: 727989-21-1
(1R,3R,6R,10R)-8-benzyloxycarbonyl-3-phenyl-8-aza-2,4-dioxabicyclo[4.4.0]decan-10-ol

Guidance literature:: With camphor-10-sulfonic acid; In chloroform; for 1h; Heating;
DOI:10.1071/CH03227

Reference yield: 88.0%

: 727989-21-1
(1R,3R,6R,10R)-8-benzyloxycarbonyl-3-phenyl-8-aza-2,4-dioxabicyclo[4.4.0]decan-10-ol

: 874-60-2
4-methyl-benzoyl chloride

: 1593576-27-2
4,5'-O-benzylidene-3-O-p-toluoyl-N-benzyloxycarbonyl-isofagomine

Guidance literature:: With pyridine; dmap; In dichloromethane; for 3h; Inert atmosphere;
DOI:10.1002/anie.201308334

Reference yield: 75.0%

: 727989-21-1
(1R,3R,6R,10R)-8-benzyloxycarbonyl-3-phenyl-8-aza-2,4-dioxabicyclo[4.4.0]decan-10-ol

: 727989-22-2
2,4,6-tri-O-acetyl-3-O-(tetra-O-acetyl-β-D-glucopyranosyl)-α-D-glucopyranosyl trichloroacetimidate

: 727989-24-4
(1R,3R,6R,10R)-8-benzyloxycarbonyl-3-phenyl-10-[(tetra-O-acetyl-β-D-glucopyranosyl)-(1->3)-O-(tri-O-acetyl-β-D-glucopyranosyl)]oxy-8-aza-2,4-dioxabicyclo[4.4.0]decane

Guidance literature:: (1R,3R,6R,10R)-8-benzyloxycarbonyl-3-phenyl-8-aza-2,4-dioxabicyclo[4.4.0]decan-10-ol; 2,4,6-tri-O-acetyl-3-O-(tetra-O-acetyl-β-D-glucopyranosyl)-α-D-glucopyranosyl trichloroacetimidate; With 4 A molecular sieve; In dichloromethane; for 2.5h;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -30 ℃; for 1h;
DOI:10.1071/CH03227