ethyl 7-(4-methoxy-3-nitrophenyl)-(2E,4E,6E)-[1,2-13C₂]hepta-2,4,6-trienoate

Base Information

Chemical Name:ethyl 7-(4-methoxy-3-nitrophenyl)-(2E,4E,6E)-[1,2-13C₂]hepta-2,4,6-trienoate
CAS No.:1026324-81-1
Molecular Formula:C₁₆H₁₇NO₅
Molecular Weight:305.293
Hs Code.:

ethyl 7-(4-methoxy-3-nitrophenyl)-(2E,4E,6E)-[1,2-13C<sub>2</sub>]hepta-2,4,6-trienoate

Synonyms:ethyl 7-(4-methoxy-3-nitrophenyl)-(2E,4E,6E)-[1,2-13C₂]hepta-2,4,6-trienoate

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Chemical Property of ethyl 7-(4-methoxy-3-nitrophenyl)-(2E,4E,6E)-[1,2-13C₂]hepta-2,4,6-trienoate

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Technology Process of ethyl 7-(4-methoxy-3-nitrophenyl)-(2E,4E,6E)-[1,2-13C₂]hepta-2,4,6-trienoate

There total 3 articles about ethyl 7-(4-methoxy-3-nitrophenyl)-(2E,4E,6E)-[1,2-13C₂]hepta-2,4,6-trienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.3%

: 100940-60-1
[¹³C₂]-triethyl phosphonoacetate

: 685523-47-1
5-(4-methoxy-3-nitrophenyl)-(2E,4E)-penta-2,4-dienal

: 1026324-81-1
ethyl 7-(4-methoxy-3-nitrophenyl)-(2E,4E,6E)-[1,2-13C₂]hepta-2,4,6-trienoate

Guidance literature:: With potassium carbonate; at 20 ℃; for 72h;
DOI:10.1021/ja039336+

Reference yield:

: (2E,4E)-5-(4-Methoxy-3-nitro-phenyl)-penta-2,4-dien-1-ol

: 1026324-81-1
ethyl 7-(4-methoxy-3-nitrophenyl)-(2E,4E,6E)-[1,2-13C₂]hepta-2,4,6-trienoate

Guidance literature:: Multi-step reaction with 2 steps

1: MnO₂

2: 67.3 percent / aq. K₂CO₃ / 72 h / 20 °C

With manganese(IV) oxide; potassium carbonate; 2: Wadsworth-Emmons reaction;
DOI:10.1021/ja039336+

Reference yield:

: ethyl 5-(4-methoxy-3-nitrophenyl)-(2E,4E)-penta-2,4-dienoate

: 1026324-81-1
ethyl 7-(4-methoxy-3-nitrophenyl)-(2E,4E,6E)-[1,2-13C₂]hepta-2,4,6-trienoate

Guidance literature:: Multi-step reaction with 3 steps

1: DIBAL-H

2: MnO₂

3: 67.3 percent / aq. K₂CO₃ / 72 h / 20 °C

With manganese(IV) oxide; diisobutylaluminium hydride; potassium carbonate; 3: Wadsworth-Emmons reaction;
DOI:10.1021/ja039336+