11-(4-chlorophenyl)-3-(4-methoxyphenyl)-7,8,9,10-tetrahydro[1,2,3]triazino[4',5':4,5]thieno[2,3-b]quinolin-4(3H)-one

Base Information

Chemical Name:11-(4-chlorophenyl)-3-(4-methoxyphenyl)-7,8,9,10-tetrahydro[1,2,3]triazino[4',5':4,5]thieno[2,3-b]quinolin-4(3H)-one
CAS No.:135747-51-2
Molecular Formula:C₂₅H₁₉ClN₄O₂S
Molecular Weight:474.97
Hs Code.:
Mol file:135747-51-2.mol

Synonyms:5-(4-Chloro-phenyl)-2-(4-methoxy-phenyl)-6,7,8,9-tetrahydro-2H-11-thia-2,3,4,10-tetraaza-benzo[b]fluoren-1-one

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Chemical Property of 11-(4-chlorophenyl)-3-(4-methoxyphenyl)-7,8,9,10-tetrahydro[1,2,3]triazino[4',5':4,5]thieno[2,3-b]quinolin-4(3H)-one

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Technology Process of 11-(4-chlorophenyl)-3-(4-methoxyphenyl)-7,8,9,10-tetrahydro[1,2,3]triazino[4',5':4,5]thieno[2,3-b]quinolin-4(3H)-one

There total 4 articles about 11-(4-chlorophenyl)-3-(4-methoxyphenyl)-7,8,9,10-tetrahydro[1,2,3]triazino[4',5':4,5]thieno[2,3-b]quinolin-4(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 135747-45-4
3-Amino-4-(4-chloro-phenyl)-5,6,7,8-tetrahydro-thieno[2,3-b]quinoline-2-carboxylic acid (4-methoxy-phenyl)-amide

: 135747-51-2
5-(4-Chloro-phenyl)-2-(4-methoxy-phenyl)-6,7,8,9-tetrahydro-2H-11-thia-2,3,4,10-tetraaza-benzo[b]fluoren-1-one

Guidance literature:: With hydrogenchloride; sodium nitrite; In acetic acid; at 0 ℃; for 0.0833333h;

Reference yield:

: 83236-51-5
2-mercapto-4-(4-chlorophenyl)-5,6,7,8-tetrahydroquinoline-3-carbonitrile

: 135747-51-2
5-(4-Chloro-phenyl)-2-(4-methoxy-phenyl)-6,7,8,9-tetrahydro-2H-11-thia-2,3,4,10-tetraaza-benzo[b]fluoren-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / NaOAc / ethanol / 2 h

2: NaOEt / ethanol / 0.25 h / Heating

3: 91 percent / 10percent NaNO₂, conc. HCl / acetic acid / 0.08 h / 0 °C

With hydrogenchloride; sodium ethanolate; sodium acetate; sodium nitrite; In ethanol; acetic acid;

Reference yield:

: 22303-36-2
N-(4-methoxyphenyl)-2-chloroacetamide

: 135747-51-2
5-(4-Chloro-phenyl)-2-(4-methoxy-phenyl)-6,7,8,9-tetrahydro-2H-11-thia-2,3,4,10-tetraaza-benzo[b]fluoren-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / NaOAc / ethanol / 2 h

2: NaOEt / ethanol / 0.25 h / Heating

3: 91 percent / 10percent NaNO₂, conc. HCl / acetic acid / 0.08 h / 0 °C

With hydrogenchloride; sodium ethanolate; sodium acetate; sodium nitrite; In ethanol; acetic acid;