(3R,4S)-3-hexyl-3-trimethylsilyl-4-<(R)-2'-3,5-(dinitrobenzoyloxy)tridecyl>-2-oxetanone

Base Information

Chemical Name:(3R,4S)-3-hexyl-3-trimethylsilyl-4-<(R)-2'-3,5-(dinitrobenzoyloxy)tridecyl>-2-oxetanone
CAS No.:161370-84-9
Molecular Formula:C₃₂H₅₂N₂O₈Si
Molecular Weight:620.859
Hs Code.:

Synonyms:(3R,4S)-3-hexyl-3-trimethylsilyl-4-<(R)-2'-3,5-(dinitrobenzoyloxy)tridecyl>-2-oxetanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R,4S)-3-hexyl-3-trimethylsilyl-4-<(R)-2'-3,5-(dinitrobenzoyloxy)tridecyl>-2-oxetanone

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Technology Process of (3R,4S)-3-hexyl-3-trimethylsilyl-4-<(R)-2'-3,5-(dinitrobenzoyloxy)tridecyl>-2-oxetanone

There total 6 articles about (3R,4S)-3-hexyl-3-trimethylsilyl-4-<(R)-2'-3,5-(dinitrobenzoyloxy)tridecyl>-2-oxetanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 161370-83-8
(3R,4S)-3-hexyl-3-trimethylsilyl-4-<(R)-2'-hydroxytridecyl>-2-oxetanone

: 99-33-2
3,5-dinitrobenoyl chloride

: 161370-84-9
(3R,4S)-3-hexyl-3-trimethylsilyl-4-<(R)-2'-3,5-(dinitrobenzoyloxy)tridecyl>-2-oxetanone

Guidance literature:: With pyridine; In tetrahydrofuran; for 2h; Ambient temperature;
DOI:10.1055/s-1994-25684

Reference yield:

: 14273-09-7
1-ethoxy-1-octyne

: 161370-84-9
(3R,4S)-3-hexyl-3-trimethylsilyl-4-<(R)-2'-3,5-(dinitrobenzoyloxy)tridecyl>-2-oxetanone

Guidance literature:: Multi-step reaction with 4 steps

1: 57 percent / I₂, Cu / 48 h / 70 °C

2: 83 percent / 1.8M EtAlCl₂ / toluene; diethyl ether / -40 - 0 °C

3: H₂ / 10percent Pd-C / tetrahydrofuran / 8 h / Ambient temperature

4: 70 percent / pyridine / tetrahydrofuran / 2 h / Ambient temperature

With pyridine; hydrogen; iodine; ethylaluminum dichloride; copper; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; toluene;
DOI:10.1055/s-1994-25684

Reference yield:

: 125564-91-2
2-Trimethylsilanyl-oct-1-en-1-one

: 161370-84-9
(3R,4S)-3-hexyl-3-trimethylsilyl-4-<(R)-2'-3,5-(dinitrobenzoyloxy)tridecyl>-2-oxetanone

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / 1.8M EtAlCl₂ / toluene; diethyl ether / -40 - 0 °C

2: H₂ / 10percent Pd-C / tetrahydrofuran / 8 h / Ambient temperature

3: 70 percent / pyridine / tetrahydrofuran / 2 h / Ambient temperature

With pyridine; hydrogen; ethylaluminum dichloride; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; toluene;
DOI:10.1055/s-1994-25684