Technology Process of C34H30N2O3
There total 6 articles about C34H30N2O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 1-naphthalenecarboxylic acid; (1R,2R)-1,2-bis[(2-diphenylphosphanyl)benzoylamino]cyclohexane;
In
tetrahydrofuran;
at 20 ℃;
for 41h;
optical yield given as %ee;
enantioselective reaction;
Inert atmosphere;
DOI:10.1021/ja209244m
- Guidance literature:
-
Multi-step reaction with 2 steps
1: rhodium(II) acetate dimer / dichloromethane / 6 h / 20 °C / Inert atmosphere
2: tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 1-naphthalenecarboxylic acid; (1R,2R)-1,2-bis[(2-diphenylphosphanyl)benzoylamino]cyclohexane / tetrahydrofuran / 41 h / 20 °C / Inert atmosphere
With
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; rhodium(II) acetate dimer; 1-naphthalenecarboxylic acid; (1R,2R)-1,2-bis[(2-diphenylphosphanyl)benzoylamino]cyclohexane;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ja209244m
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium tert-butylate / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere
2: tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 1-naphthalenecarboxylic acid; (1R,2R)-1,2-bis[(2-diphenylphosphanyl)benzoylamino]cyclohexane / tetrahydrofuran / 41 h / 20 °C / Inert atmosphere
With
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 1-naphthalenecarboxylic acid; potassium tert-butylate; (1R,2R)-1,2-bis[(2-diphenylphosphanyl)benzoylamino]cyclohexane;
In
tetrahydrofuran;
DOI:10.1021/ja209244m
