tert-butyl 2-benzoyl-2-(diphenylmethyleneamino)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanoate

Base Information

Chemical Name:tert-butyl 2-benzoyl-2-(diphenylmethyleneamino)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanoate
CAS No.:1345673-17-7
Molecular Formula:C₃₆H₄₄BNO₅
Molecular Weight:581.56
Hs Code.:

Synonyms:tert-butyl 2-benzoyl-2-(diphenylmethyleneamino)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanoate

Suppliers and Price of tert-butyl 2-benzoyl-2-(diphenylmethyleneamino)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of tert-butyl 2-benzoyl-2-(diphenylmethyleneamino)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanoate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of tert-butyl 2-benzoyl-2-(diphenylmethyleneamino)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanoate

There total 3 articles about tert-butyl 2-benzoyl-2-(diphenylmethyleneamino)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1345673-16-6
tert-butyl 2-benzoyl-2-(diphenylmethyleneamino)hex-5-enoate

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1345673-17-7
tert-butyl 2-benzoyl-2-(diphenylmethyleneamino)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanoate

Guidance literature:: tert-butyl 2-benzoyl-2-(diphenylmethyleneamino)hex-5-enoate; bis(1,5-cyclooctadiene)diiridium(I) dichloride; 1,2-bis-(diphenylphosphino)ethane; In dichloromethane; at 20 ℃; for 0.5h;

4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; In dichloromethane;

Reference yield:

: 81477-94-3
N-(diphenylmethylene)glycine tert-butyl ester

: 1345673-17-7
tert-butyl 2-benzoyl-2-(diphenylmethyleneamino)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C

2.2: 1.5 h / -78 - 20 °C

3.1: bis(1,5-cyclooctadiene)diiridium(I) dichloride; 1,2-bis-(diphenylphosphino)ethane / dichloromethane / 0.5 h / 20 °C

With sodium hexamethyldisilazane; bis(1,5-cyclooctadiene)diiridium(I) dichloride; 1,2-bis-(diphenylphosphino)ethane; In tetrahydrofuran; dichloromethane;

Reference yield:

: 936116-57-3
N-(diphenylmethylene)-DL-homoallylglycine tert-butyl ester

: 1345673-17-7
tert-butyl 2-benzoyl-2-(diphenylmethyleneamino)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C

1.2: 1.5 h / -78 - 20 °C

2.1: bis(1,5-cyclooctadiene)diiridium(I) dichloride; 1,2-bis-(diphenylphosphino)ethane / dichloromethane / 0.5 h / 20 °C

With sodium hexamethyldisilazane; bis(1,5-cyclooctadiene)diiridium(I) dichloride; 1,2-bis-(diphenylphosphino)ethane; In tetrahydrofuran; dichloromethane;