3,4,5-Tribromo-1-{2-[4-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-phenyl]-ethyl}-1H-pyrrole-2-carbonyl chloride

Base Information

Chemical Name:3,4,5-Tribromo-1-{2-[4-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-phenyl]-ethyl}-1H-pyrrole-2-carbonyl chloride
CAS No.:86288-72-4
Molecular Formula:C₂₁H₁₂Br₃ClN₂O₃
Molecular Weight:615.503
Hs Code.:

Synonyms:3,4,5-Tribromo-1-{2-[4-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-phenyl]-ethyl}-1H-pyrrole-2-carbonyl chloride

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Chemical Property of 3,4,5-Tribromo-1-{2-[4-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-phenyl]-ethyl}-1H-pyrrole-2-carbonyl chloride

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Technology Process of 3,4,5-Tribromo-1-{2-[4-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-phenyl]-ethyl}-1H-pyrrole-2-carbonyl chloride

There total 4 articles about 3,4,5-Tribromo-1-{2-[4-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-phenyl]-ethyl}-1H-pyrrole-2-carbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 86288-64-4
3,4,5-Tribromo-1-{2-[4-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-phenyl]-ethyl}-1H-pyrrole-2-carboxylic acid

: 86288-72-4
3,4,5-Tribromo-1-{2-[4-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-phenyl]-ethyl}-1H-pyrrole-2-carbonyl chloride

Guidance literature:: With Dichloromethyl methyl ether; for 0.5h; Heating;
DOI:10.1021/jo00167a015

Reference yield:

: 1198-67-0
methyl 3,4,5-tribromo-1H-pyrrole-2-carboxylate

: 86288-72-4
3,4,5-Tribromo-1-{2-[4-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-phenyl]-ethyl}-1H-pyrrole-2-carbonyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / K₂CO₃ / dimethylformamide / 4 h / 85 °C

2: 100 percent / 6 N NaOH / ethanol / 2 h / Heating

3: 98 percent / Dichloromethyl methyl ether / 0.5 h / Heating

With sodium hydroxide; Dichloromethyl methyl ether; potassium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo00167a015

Reference yield:

: 86288-78-0
p-Phthalimidophenethyl mesylate

: 86288-72-4
3,4,5-Tribromo-1-{2-[4-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-phenyl]-ethyl}-1H-pyrrole-2-carbonyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / K₂CO₃ / dimethylformamide / 4 h / 85 °C

2: 100 percent / 6 N NaOH / ethanol / 2 h / Heating

3: 98 percent / Dichloromethyl methyl ether / 0.5 h / Heating

With sodium hydroxide; Dichloromethyl methyl ether; potassium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo00167a015