5-methyl-2,3-di-p-tolyl-1,3,4-oxadiazol-3-ium trifluoromethanesulfonate

Base Information

Chemical Name:5-methyl-2,3-di-p-tolyl-1,3,4-oxadiazol-3-ium trifluoromethanesulfonate
CAS No.:1443786-91-1
Molecular Formula:CF₃O₃S*C₁₇H₁₇N₂O
Molecular Weight:414.405
Hs Code.:

Synonyms:5-methyl-2,3-di-p-tolyl-1,3,4-oxadiazol-3-ium trifluoromethanesulfonate

Suppliers and Price of 5-methyl-2,3-di-p-tolyl-1,3,4-oxadiazol-3-ium trifluoromethanesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-methyl-2,3-di-p-tolyl-1,3,4-oxadiazol-3-ium trifluoromethanesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-methyl-2,3-di-p-tolyl-1,3,4-oxadiazol-3-ium trifluoromethanesulfonate

There total 3 articles about 5-methyl-2,3-di-p-tolyl-1,3,4-oxadiazol-3-ium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1493-13-6
trifluorormethanesulfonic acid

: 24660-34-2
N'-acetyl-4-methyl-N-(p-tolyl)benzohydrazide

: 1443786-91-1
5-methyl-2,3-di-p-tolyl-1,3,4-oxadiazol-3-ium trifluoromethanesulfonate

Guidance literature:: With acetic anhydride; In water; at 23 ℃; Inert atmosphere;
DOI:10.1055/s-0032-1316877

Reference yield:

: 61700-79-6
N'-(4-methylphenyl)acetohydrazide

: 1443786-91-1
5-methyl-2,3-di-p-tolyl-1,3,4-oxadiazol-3-ium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 5 h / 80 °C / Inert atmosphere

2: acetic anhydride / water / 23 °C / Inert atmosphere

With acetic anhydride; In water; toluene;
DOI:10.1055/s-0032-1316877

Reference yield:

: 637-60-5,35467-65-3
p-tolylhydrazine hydrochloride

: 1443786-91-1
5-methyl-2,3-di-p-tolyl-1,3,4-oxadiazol-3-ium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 14 h / 20 °C / Inert atmosphere

2: toluene / 5 h / 80 °C / Inert atmosphere

3: acetic anhydride / water / 23 °C / Inert atmosphere

With acetic anhydride; triethylamine; In dichloromethane; water; toluene;
DOI:10.1055/s-0032-1316877