dimethyl[(2-methoxy-9,10-dihydro-3-phenanthryl)methyl][(phenylthio)methyl]ammonium bromide

Base Information

Chemical Name:dimethyl[(2-methoxy-9,10-dihydro-3-phenanthryl)methyl][(phenylthio)methyl]ammonium bromide
CAS No.:97860-91-8
Molecular Formula:Br*C₂₅H₂₈NOS
Molecular Weight:470.473
Hs Code.:

Synonyms:dimethyl[(2-methoxy-9,10-dihydro-3-phenanthryl)methyl][(phenylthio)methyl]ammonium bromide

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Chemical Property of dimethyl[(2-methoxy-9,10-dihydro-3-phenanthryl)methyl][(phenylthio)methyl]ammonium bromide

Chemical Property:

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Technology Process of dimethyl[(2-methoxy-9,10-dihydro-3-phenanthryl)methyl][(phenylthio)methyl]ammonium bromide

There total 3 articles about dimethyl[(2-methoxy-9,10-dihydro-3-phenanthryl)methyl][(phenylthio)methyl]ammonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 43180-39-8
dimethyl<(phenylthio)methyl>amine

: 97860-90-7
3-(bromomethyl)-2-methoxy-9,10-dihydrophenanthrene

: 97860-91-8
dimethyl[(2-methoxy-9,10-dihydro-3-phenanthryl)methyl][(phenylthio)methyl]ammonium bromide

Guidance literature:: In acetonitrile; at 25 ℃; for 16h;
DOI:10.1021/jm00148a031

Reference yield:

: 85531-84-6
Methyl 2-methoxy-9,10-dihydrophenanthrene-3-carboxylate

: 97860-91-8
dimethyl[(2-methoxy-9,10-dihydro-3-phenanthryl)methyl][(phenylthio)methyl]ammonium bromide

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / LiAlH₄ / tetrahydrofuran / 1.5 h / 0 °C

2: 88 percent / HBr (gas) / benzene / 0.5 h / 25 °C

3: 100 percent / acetonitrile / 16 h / 25 °C

With lithium aluminium tetrahydride; hydrogen bromide; In tetrahydrofuran; acetonitrile; benzene;
DOI:10.1021/jm00148a031

Reference yield:

: 97860-89-4
3-(hydroxymethyl)-2-methoxy-9,10-dihydrophenanthrene

: 97860-91-8
dimethyl[(2-methoxy-9,10-dihydro-3-phenanthryl)methyl][(phenylthio)methyl]ammonium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / HBr (gas) / benzene / 0.5 h / 25 °C

2: 100 percent / acetonitrile / 16 h / 25 °C

With hydrogen bromide; In acetonitrile; benzene;
DOI:10.1021/jm00148a031