C₇₀H₉₈O₉Si₃

Base Information

Chemical Name:C₇₀H₉₈O₉Si₃
CAS No.:1261152-35-5
Molecular Formula:C₇₀H₉₈O₉Si₃
Molecular Weight:1167.8
Hs Code.:

C<sub>70</sub>H<sub>98</sub>O<sub>9</sub>Si<sub>3</sub>

Synonyms:C₇₀H₉₈O₉Si₃

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Chemical Property of C₇₀H₉₈O₉Si₃

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Technology Process of C₇₀H₉₈O₉Si₃

There total 38 articles about C₇₀H₉₈O₉Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1261152-34-4
C₇₁H₁₀₀O₉SSi₃

: 75-24-1
trimethylaluminum

: 1261152-35-5
C₇₀H₉₈O₉Si₃

Guidance literature:: C₇₁H₁₀₀O₉SSi₃; With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 - 30 ℃; Inert atmosphere;

trimethylaluminum; In hexane; dichloromethane; at -78 - 0 ℃; Inert atmosphere;
DOI:10.1021/ja109533y

Reference yield: 100.0%

: 1261152-58-2
C₇₁H₁₀₀O₉SSi₃

: 75-24-1
trimethylaluminum

: 1261152-35-5
C₇₀H₉₈O₉Si₃

Guidance literature:: C₇₁H₁₀₀O₉SSi₃; With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 - 0 ℃; for 4.5h; Inert atmosphere;

trimethylaluminum; In hexane; dichloromethane; at -40 ℃; for 0.333333h; Inert atmosphere;
DOI:10.1021/ja109533y

Reference yield:

: 1261152-23-1
C₃₁H₄₈O₅Si₂

: 1261152-35-5
C₇₀H₉₈O₉Si₃

Guidance literature:: Multi-step reaction with 23 steps

1.1: dichloromethane / 1.5 h / 25 °C / Inert atmosphere

2.1: 2,6-dimethylpyridine / dichloromethane / 14 h / 0 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / dichloromethane / 1 h / -78 °C / Inert atmosphere

3.2: 16 h / 25 °C / Inert atmosphere

4.1: titanium(IV) isopropylate; diethyl (2S,3S)-tartrate / dichloromethane / 1 h / -25 °C / Inert atmosphere; Molecular sieve

4.2: 17 h / -20 °C / Inert atmosphere; Molecular sieve

5.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 0 - 25 °C / Inert atmosphere

6.1: dichloromethane / 14 h / 20 °C / Inert atmosphere

7.1: tetrabutyl ammonium fluoride / dichloromethane / 0.33 h / 0 °C / Inert atmosphere

8.1: pyridinium p-toluenesulfonate / dichloromethane / 25 - 40 °C / Inert atmosphere

9.1: lanthanum(lll) triflate / toluene / 6 h / 25 °C / Inert atmosphere

10.1: sodium tetrahydroborate; nickel (II) chloride hexahydrate / ethanol / 0 °C / Inert atmosphere

11.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 0.5 h / 25 °C / Inert atmosphere

12.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 0 - 25 °C / Inert atmosphere

13.1: sodium hexamethyldisilazane / tetrahydrofuran; toluene / 0.17 h / 0 °C / Inert atmosphere

13.2: 0.33 h / 0 °C / Inert atmosphere

14.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 3 h / 0 °C / Inert atmosphere

15.1: dmap; 2-methyl-6-nitrobenzoic anhydride; triethylamine / toluene / 0.33 h / 25 °C / Inert atmosphere; Molecular sieve

15.2: 13 h / 25 °C / Inert atmosphere; Molecular sieve

16.1: p-toluenesulfonic acid monohydrate / methanol; dichloromethane / 0.67 h / 0 °C / Inert atmosphere

17.1: N,N,N,N,-tetramethylethylenediamine; titanium tetrachloride / tetrahydrofuran; dichloromethane / 0 - 25 °C / Inert atmosphere

17.2: 0.67 h / 25 °C / Inert atmosphere

18.1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 °C / Inert atmosphere

19.1: bis(cyclohexanyl)borane / tetrahydrofuran / 6 h / 25 °C / Inert atmosphere

19.2: 20 h / 0 °C / Inert atmosphere

20.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0 - 25 °C / Inert atmosphere

21.1: p-toluenesulfonic acid monohydrate / methanol; dichloromethane / 0.5 h / 0 °C / Inert atmosphere

22.1: zinc trifluoromethanesulfonate / dichloromethane / 16 h / 25 °C / Inert atmosphere

23.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / -78 - 30 °C / Inert atmosphere

23.2: -78 - 0 °C / Inert atmosphere

With 2,6-dimethylpyridine; titanium(IV) isopropylate; dmap; sodium tetrahydroborate; lithium aluminium tetrahydride; nickel (II) chloride hexahydrate; diethyl (2S,3S)-tartrate; N,N,N,N,-tetramethylethylenediamine; bis(cyclohexanyl)borane; 2-methyl-6-nitrobenzoic anhydride; p-toluenesulfonic acid monohydrate; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; pyridinium p-toluenesulfonate; titanium tetrachloride; zinc trifluoromethanesulfonate; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; dimethyl sulfoxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lanthanum(lll) triflate; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; toluene; 1.1: Wittig reaction / 4.1: Sharpless epoxidation / 4.2: Sharpless epoxidation / 5.1: Parikh-Doering oxidation / 6.1: Wittig reaction / 12.1: Parikh-Doering oxidation / 13.1: Wittig reaction / 13.2: Wittig reaction / 19.1: Hydroboration reaction;
DOI:10.1021/ja109533y