N,N'-bis(2-aminothiophenol)-α,α'-bis(5-bromocarboxylidenephenoxy)-1,4-xylene

Base Information

Chemical Name:N,N'-bis(2-aminothiophenol)-α,α'-bis(5-bromocarboxylidenephenoxy)-1,4-xylene
CAS No.:1329993-36-3
Molecular Formula:C₃₄H₂₆Br₂N₂O₂S₂
Molecular Weight:718.533
Hs Code.:

Synonyms:N,N'-bis(2-aminothiophenol)-α,α'-bis(5-bromocarboxylidenephenoxy)-1,4-xylene

Suppliers and Price of N,N'-bis(2-aminothiophenol)-α,α'-bis(5-bromocarboxylidenephenoxy)-1,4-xylene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-bis(2-aminothiophenol)-α,α'-bis(5-bromocarboxylidenephenoxy)-1,4-xylene

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Technology Process of N,N'-bis(2-aminothiophenol)-α,α'-bis(5-bromocarboxylidenephenoxy)-1,4-xylene

There total 2 articles about N,N'-bis(2-aminothiophenol)-α,α'-bis(5-bromocarboxylidenephenoxy)-1,4-xylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1329993-34-1
α,α'-bis(5-bromo-2-carboxyaldehydephenoxy)-1,4-xylene

: 137-07-5
2-amino-benzenethiol

: 1329993-36-3
N,N'-bis(2-aminothiophenol)-α,α'-bis(5-bromocarboxylidenephenoxy)-1,4-xylene

Guidance literature:: In ethanol; for 2h;
DOI:10.1016/j.saa.2011.05.087

Reference yield:

: 623-24-5
1,4-bis(bromomethyl)benzene

: 22532-62-3
4-bromosalicylaldehyde

: 1329993-36-3
N,N'-bis(2-aminothiophenol)-α,α'-bis(5-bromocarboxylidenephenoxy)-1,4-xylene

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 8 h / 20 - 155 °C

2: ethanol / 2 h

With potassium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.saa.2011.05.087