(4,4'-dihexyl-cyclopenta[2,1-b:3,4-b']dithiophene-2-carbaldehyde)phenylazanediyldibenzoic acid

Base Information

Chemical Name:(4,4'-dihexyl-cyclopenta[2,1-b:3,4-b']dithiophene-2-carbaldehyde)phenylazanediyldibenzoic acid
CAS No.:1350734-26-7
Molecular Formula:C₄₂H₄₃NO₅S₂
Molecular Weight:705.939
Hs Code.:

Synonyms:(4,4'-dihexyl-cyclopenta[2,1-b:3,4-b']dithiophene-2-carbaldehyde)phenylazanediyldibenzoic acid

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Chemical Property of (4,4'-dihexyl-cyclopenta[2,1-b:3,4-b']dithiophene-2-carbaldehyde)phenylazanediyldibenzoic acid

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Technology Process of (4,4'-dihexyl-cyclopenta[2,1-b:3,4-b']dithiophene-2-carbaldehyde)phenylazanediyldibenzoic acid

There total 3 articles about (4,4'-dihexyl-cyclopenta[2,1-b:3,4-b']dithiophene-2-carbaldehyde)phenylazanediyldibenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1332724-76-1
C₅₀H₅₉NO₅S₂

: 1350734-26-7
(4,4'-dihexyl-cyclopenta[2,1-b:3,4-b']dithiophene-2-carbaldehyde)phenylazanediyldibenzoic acid

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ol202014x

Reference yield:

: N,N-di(4-benzoic acid tert-butyl ester)-4-(5’-(4,4,5,5-tetramethyl-[1,3,2]dioxoborolane-2-yl)-4,3’dihexyl-2,2’-bithien-5-yl)phenylamine

: 1350734-26-7
(4,4'-dihexyl-cyclopenta[2,1-b:3,4-b']dithiophene-2-carbaldehyde)phenylazanediyldibenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / ethanol; water; toluene / 24 h / 95 °C / Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 12 h / 20 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; trifluoroacetic acid; In ethanol; dichloromethane; water; toluene; 1: Suzuki coupling;
DOI:10.1021/ol202014x

Reference yield:

: 1221821-39-1
6-bromo-4,4-dihexyl-4H-cyclopenta[2,1-b:3,4-b′]dithiophene-2-carbaldehyde

: 1350734-26-7
(4,4'-dihexyl-cyclopenta[2,1-b:3,4-b']dithiophene-2-carbaldehyde)phenylazanediyldibenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / ethanol; water; toluene / 24 h / 95 °C / Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 12 h / 20 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; trifluoroacetic acid; In ethanol; dichloromethane; water; toluene; 1: Suzuki coupling;
DOI:10.1021/ol202014x