4-N-benzoyl-1-cytosine

Base Information

Chemical Name:4-N-benzoyl-1-cytosine
CAS No.:112302-53-1
Molecular Formula:C₄₂H₃₇N₅O₁₁
Molecular Weight:787.783
Hs Code.:

4-N-benzoyl-1-<methyl-3,7-anhydro-2-O-benzoyl-5-(3-N-benzoylureido)-6-O-benzyl-5-deoxy-α-L-erythro-D-allooctofuranos-(1,4)-yluronate>cytosine

Synonyms:4-N-benzoyl-1-cytosine

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Chemical Property of 4-N-benzoyl-1-cytosine

Chemical Property:

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Technology Process of 4-N-benzoyl-1-cytosine

There total 15 articles about 4-N-benzoyl-1-cytosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-<8-O-allyl-3,7-anhydro-6-O-benzyl-5-deoxy-5-ureido-α-L-erythro-D-allooctofuranos-(1,4)-yl>cytosine

: 112302-53-1
4-N-benzoyl-1-cytosine

Guidance literature:: Multi-step reaction with 5 steps

1: 62 percent / pyridine / 1 h / ice cooling

2: 73 percent / selenium dioxide, acetic acid / dioxane / 0.75 h / Heating

3: Jones' reagent / acetone / 1 h / ice cooling

4: 5percent HCl / 1 h / Heating

5: pyridine / 0.25 h / ice cooling

With pyridine; hydrogenchloride; selenium(IV) oxide; jones' reagent; acetic acid; In 1,4-dioxane; acetone;
DOI:10.1246/bcsj.60.1057

Reference yield:

: 1-((2R,3R,3aS,5S,6R,7R,7aR)-5-Allyloxymethyl-7-amino-6-benzyloxy-3-hydroxy-hexahydro-furo[3,2-b]pyran-2-yl)-4-amino-3,4-dihydro-1H-pyrimidin-2-one

: 112302-53-1
4-N-benzoyl-1-cytosine

Guidance literature:: Multi-step reaction with 6 steps

1: 30percent acetic acid / H₂O / 10 h / 50 °C

2: 62 percent / pyridine / 1 h / ice cooling

3: 73 percent / selenium dioxide, acetic acid / dioxane / 0.75 h / Heating

4: Jones' reagent / acetone / 1 h / ice cooling

5: 5percent HCl / 1 h / Heating

6: pyridine / 0.25 h / ice cooling

With pyridine; hydrogenchloride; selenium(IV) oxide; jones' reagent; acetic acid; In 1,4-dioxane; water; acetone;
DOI:10.1246/bcsj.60.1057

Reference yield:

: 1-<8-O-allyl-3,7-anhydro-6-O-benzyl-5-deoxy-5-(2,4-dinitrophenylamino)-α-L-erythro-D-allooctofuranos-(1,4)-yl>-uracil

: 112302-53-1
4-N-benzoyl-1-cytosine

Guidance literature:: Multi-step reaction with 10 steps

1: 98.2 percent / pyridine / 1 h / ice cooling

2: oxalyl dichloride, DMF / 1,2-dichloro-ethane / 36 h / Ambient temperature

3: NH₃ / methanol / 5 h / Ambient temperature

4: Amberlite IRA-400(OH-) / acetone; methanol; H₂O / 3 h / Heating

5: 30percent acetic acid / H₂O / 10 h / 50 °C

6: 62 percent / pyridine / 1 h / ice cooling

7: 73 percent / selenium dioxide, acetic acid / dioxane / 0.75 h / Heating

8: Jones' reagent / acetone / 1 h / ice cooling

9: 5percent HCl / 1 h / Heating

10: pyridine / 0.25 h / ice cooling

With pyridine; hydrogenchloride; selenium(IV) oxide; jones' reagent; oxalyl dichloride; Amberlite IRA-400(OH-); ammonia; acetic acid; N,N-dimethyl-formamide; In 1,4-dioxane; methanol; water; 1,2-dichloro-ethane; acetone;
DOI:10.1246/bcsj.60.1057