Technology Process of C33H45N3O7
There total 8 articles about C33H45N3O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C25H37IN2O5; C8H10BNO4;
With
potassium acetate; caesium carbonate;
In
dimethyl sulfoxide;
for 0.166667h;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
dimethyl sulfoxide;
at 70 ℃;
for 10.5h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: trimethylaluminum / hexane; dichloromethane / 0.25 h
1.2: 20 °C
1.3: 2 h
2.1: potassium acetate; caesium carbonate / dimethyl sulfoxide / 0.17 h
2.2: 10.5 h / 70 °C
With
trimethylaluminum; potassium acetate; caesium carbonate;
In
hexane; dichloromethane; dimethyl sulfoxide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: benzene / Heating / reflux
2.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation
2.2: 2 h
3.1: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 4 h / 20 °C
4.1: trimethylaluminum / hexane; dichloromethane / 0.25 h
4.2: 20 °C
4.3: 2 h
5.1: potassium acetate; caesium carbonate / dimethyl sulfoxide / 0.17 h
5.2: 10.5 h / 70 °C
With
titanium(IV) isopropylate; trimethylaluminum; potassium acetate; caesium carbonate; pyridine hydrogenfluoride;
In
tetrahydrofuran; pyridine; hexane; dichloromethane; dimethyl sulfoxide; toluene; benzene;
