N^α-<(9-fluorenylmethyl)oxy>carbonyl-N^ε-(tert-butyloxycarbonyl)-D-lysyl-N-methylleucyl-N-methylleucyl-N-methylvalyl-(2S,3R,4R,6E)-3-hydroxy-4-methyl-2-(methylamino)-6-octenoyl-L-2-aminobutyrylsarcosyl-N-methylleucylvalyl-N-methylleucylalanyl ben...

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• Chemical Name: N^α-<(9-fluorenylmethyl)oxy>carbonyl-N^ε-(tert-butyloxycarbonyl)-D-lysyl-N-methylleucyl-N-methylleucyl-N-methylvalyl-(2S,3R,4R,6E)-3-hydroxy-4-methyl-2-(methylamino)-6-octenoyl-L-2-aminobutyrylsarcosyl-N-methylleucylvalyl-N-methylleucylalanyl ben...
• CAS No.: 104186-79-0
• Molecular Formula: C₉₂H₁₄₄N₁₂O₁₇
• Molecular Weight: 1690.23

Synonyms:N^α-<(9-fluorenylmethyl)oxy>carbonyl-N^ε-(tert-butyloxycarbonyl)-D-lysyl-N-methylleucyl-N-methylleucyl-N-methylvalyl-(2S,3R,4R,6E)-3-hydroxy-4-methyl-2-(methylamino)-6-octenoyl-L-2-aminobutyrylsarcosyl-N-methylleucylvalyl-N-methylleucylalanyl ben...

Chemical Property of N^α-<(9-fluorenylmethyl)oxy>carbonyl-N^ε-(tert-butyloxycarbonyl)-D-lysyl-N-methylleucyl-N-methylleucyl-N-methylvalyl-(2S,3R,4R,6E)-3-hydroxy-4-methyl-2-(methylamino)-6-octenoyl-L-2-aminobutyrylsarcosyl-N-methylleucylvalyl-N-methylleucylalanyl ben...

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Technology Process of N^α-<(9-fluorenylmethyl)oxy>carbonyl-N^ε-(tert-butyloxycarbonyl)-D-lysyl-N-methylleucyl-N-methylleucyl-N-methylvalyl-(2S,3R,4R,6E)-3-hydroxy-4-methyl-2-(methylamino)-6-octenoyl-L-2-aminobutyrylsarcosyl-N-methylleucylvalyl-N-methylleucylalanyl ben...

There total 1 articles about N^α-<(9-fluorenylmethyl)oxy>carbonyl-N^ε-(tert-butyloxycarbonyl)-D-lysyl-N-methylleucyl-N-methylleucyl-N-methylvalyl-(2S,3R,4R,6E)-3-hydroxy-4-methyl-2-(methylamino)-6-octenoyl-L-2-aminobutyrylsarcosyl-N-methylleucylvalyl-N-methylleucylalanyl ben... which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

Nα-<(9-fluorenylmethyl)oxy>carbonyl-Nε-(tert-butyloxycarbonyl)-D-lysyl-N-methylleucyl-N-methylleucyl-N-methylvaline (104186-80-3) + (2S,3R,4R,6E)-3-hydroxy-4-methyl-2-(methylamino)-6-octenoyl-L-2-aminobutyrylsarcosyl-N-methylleucylvalyl-N-methylleucylalanine benzyl ester (81135-33-3) → Nα-<(9-fluorenylmethyl)oxy>carbonyl-Nε-(tert-butyloxycarbonyl)-D-lysyl-N-methylleucyl-N-methylleucyl-N-methylvalyl-(2S,3R,4R,6E)-3-hydroxy-4-methyl-2-(methylamino)-6-octenoyl-L-2-aminobutyrylsarcosyl-N-methylleucylvalyl-N-methylleucylalanyl ben... (104186-79-0)

Guidance literature:

With 4-methyl-morpholine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; In dichloromethane; for 72h; Ambient temperature;

DOI:10.1021/jo00296a061

upstream raw materials:

N^α-<(9-fluorenylmethyl)oxy>carbonyl-N^ε-(tert-butyloxycarbonyl)-D-lysyl-N-methylleucyl-N-methylleucyl-N-methylvaline

(2S,3R,4R,6E)-3-hydroxy-4-methyl-2-(methylamino)-6-octenoyl-L-2-aminobutyrylsarcosyl-N-methylleucylvalyl-N-methylleucylalanine benzyl ester

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