2(C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*CrFe₃(CO)13C^(2-)={(C₆H₅)3PNP(C₆H₅)3}2{CrFe₃(CO)13C}

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Chemical Name:2(C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*CrFe₃(CO)13C^(2-)={(C₆H₅)3PNP(C₆H₅)3}2{CrFe₃(CO)13C}
CAS No.:88669-42-5
Molecular Formula:C₁₄CrFe₃O₁₃*2C₃₆H₃₀NP₂
Molecular Weight:1672.86
Hs Code.:

2(C<sub>6</sub>H<sub>5</sub>)3PNP(C<sub>6</sub>H<sub>5</sub>)3<sup>(1+)</sup>*CrFe<sub>3</sub>(CO)13C<sup>(2-)</sup>={(C<sub>6</sub>H<sub>5</sub>)3PNP(C<sub>6</sub>H<sub>5</sub>)3}2{CrFe<sub>3</sub>(CO)13C}

Synonyms:2(C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*CrFe₃(CO)13C^(2-)={(C₆H₅)3PNP(C₆H₅)3}2{CrFe₃(CO)13C}

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Chemical Property of 2(C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*CrFe₃(CO)13C^(2-)={(C₆H₅)3PNP(C₆H₅)3}2{CrFe₃(CO)13C}

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Technology Process of 2(C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*CrFe₃(CO)13C^(2-)={(C₆H₅)3PNP(C₆H₅)3}2{CrFe₃(CO)13C}

There total 2 articles about 2(C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*CrFe₃(CO)13C^(2-)={(C₆H₅)3PNP(C₆H₅)3}2{CrFe₃(CO)13C} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 2[(C₆H₅)3PNP(C₆H₅)3]⁽¹⁺⁾*[Fe₃(CO)9(CCO)]^(2-)=[(C₆H₅)3PNP(C₆H₅)3]2[Fe₃(CO)9(CCO)]

: 16800-46-7,22736-49-8
trisacetonitrile(tricarbonyl)chromium⁽⁰⁾

: 88669-42-5
2(C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*CrFe₃(CO)13C^(2-)={(C₆H₅)3PNP(C₆H₅)3}2{CrFe₃(CO)13C}

Guidance literature:: In isopropyl alcohol; acetone; under N2, the flask with educts was immersed in a -23°C (CCl4 slush) cold bath and acetone was slowly added, the soln. was stirred 30 min and then 2-propanol added, the cold bath was removed and mixt. was heated to room temp.; ppt. was filtered, washed with methanol and Et2O, dried in vac., recrystd. from CH2Cl2; elem.anal.;

Reference yield:

: 16800-46-7,22736-49-8
trisacetonitrile(tricarbonyl)chromium⁽⁰⁾

: C₁₁Fe₃O₁₀^(2-)

: 88669-42-5
Fe₃(CO)9CCr(CO)4^(2-)*2(C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾

Guidance literature:: With (C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾; In not given; -20°C;; elem. anal.;;
DOI:10.1021/om00081a031

Reference yield: 74.0%

: 88669-42-5
2(C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*CrFe₃(CO)13C^(2-)={(C₆H₅)3PNP(C₆H₅)3}2{CrFe₃(CO)13C}

: 112680-35-0
(C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*CrFe₃(CO)13CH^(1-)={(C₆H₅)3PNP(C₆H₅)3}{CrFe₃(CO)13CH}

Guidance literature:: With HSO₃CF₃; In dichloromethane; -78 °C, after 10 min. slowly warmed up to room temp., evaporated to dryness, residue was extracted with Et2O, filtration; crystn. from 2-PrOH/pentane; elemental analysis;