methyl 4-(2-amino-4,6-dioxo-4,5,6,7-tetrahydro-3H-pyrrolo[2,3-d]pyrimidin-5-ylmethyl)-benzoate

Base Information

Chemical Name:methyl 4-(2-amino-4,6-dioxo-4,5,6,7-tetrahydro-3H-pyrrolo[2,3-d]pyrimidin-5-ylmethyl)-benzoate
CAS No.:1320346-42-6
Molecular Formula:C₁₅H₁₄N₄O₄
Molecular Weight:314.301
Hs Code.:

Synonyms:methyl 4-(2-amino-4,6-dioxo-4,5,6,7-tetrahydro-3H-pyrrolo[2,3-d]pyrimidin-5-ylmethyl)-benzoate

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Chemical Property of methyl 4-(2-amino-4,6-dioxo-4,5,6,7-tetrahydro-3H-pyrrolo[2,3-d]pyrimidin-5-ylmethyl)-benzoate

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Technology Process of methyl 4-(2-amino-4,6-dioxo-4,5,6,7-tetrahydro-3H-pyrrolo[2,3-d]pyrimidin-5-ylmethyl)-benzoate

There total 2 articles about methyl 4-(2-amino-4,6-dioxo-4,5,6,7-tetrahydro-3H-pyrrolo[2,3-d]pyrimidin-5-ylmethyl)-benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1320346-36-8
C₁₁H₁₀Br₂O₃

: 56-06-4
2,6-diaminopyrimidin-4-ol

: 1320346-42-6
methyl 4-(2-amino-4,6-dioxo-4,5,6,7-tetrahydro-3H-pyrrolo[2,3-d]pyrimidin-5-ylmethyl)-benzoate

Guidance literature:: C₁₁H₁₀Br₂O₃; 2,6-diaminopyrimidin-4-ol; In water; acetonitrile; for 0.0833333h;

With sodium acetate; In water; acetonitrile; Reflux;
DOI:10.1016/j.tetlet.2011.05.141

Reference yield:

: 113100-81-5
4-(3-oxo-propyl)-benzoic acid methyl ester

: 1320346-42-6
methyl 4-(2-amino-4,6-dioxo-4,5,6,7-tetrahydro-3H-pyrrolo[2,3-d]pyrimidin-5-ylmethyl)-benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogen bromide; bromine; acetic acid / dichloromethane / Reflux

2.1: water; acetonitrile / 0.08 h

2.2: Reflux

With hydrogen bromide; bromine; acetic acid; In dichloromethane; water; acetonitrile;
DOI:10.1016/j.tetlet.2011.05.141