(2S,3S)-3-hydroxy-2-methyl-3-(1-phenylsulfanylcyclopentyl)propyl-N-tosylamide

Base Information

Chemical Name:(2S,3S)-3-hydroxy-2-methyl-3-(1-phenylsulfanylcyclopentyl)propyl-N-tosylamide
CAS No.:138650-00-7
Molecular Formula:C₂₂H₂₉NO₃S₂
Molecular Weight:419.609
Hs Code.:

Synonyms:(2S,3S)-3-hydroxy-2-methyl-3-(1-phenylsulfanylcyclopentyl)propyl-N-tosylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S)-3-hydroxy-2-methyl-3-(1-phenylsulfanylcyclopentyl)propyl-N-tosylamide

Chemical Property:

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Technology Process of (2S,3S)-3-hydroxy-2-methyl-3-(1-phenylsulfanylcyclopentyl)propyl-N-tosylamide

There total 4 articles about (2S,3S)-3-hydroxy-2-methyl-3-(1-phenylsulfanylcyclopentyl)propyl-N-tosylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 138649-99-7
(2S,3S)-3-hydroxy-2-methyl-3-(1-phenylsulfanylcyclopentyl)propylamine

: 98-59-9
p-toluenesulfonyl chloride

: 138650-00-7
(2S,3S)-3-hydroxy-2-methyl-3-(1-phenylsulfanylcyclopentyl)propyl-N-tosylamide

Guidance literature:: With dmap;
DOI:10.1016/0040-4039(91)80244-Z

Reference yield:

: 115205-40-8
1-phenylsulfanylcyclopentane carboxaldehyde

: 138650-00-7
(2S,3S)-3-hydroxy-2-methyl-3-(1-phenylsulfanylcyclopentyl)propyl-N-tosylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) dibutylboron trifluoromethanesulfonate, diisopropylethylamine / 1.) CH₂Cl₂, 0 deg C, 1 h, 2.) CH₂Cl₂, -78 deg C (1 h), room temp. (5 h)

With di-n-butylboryl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine;

Reference yield:

: 138649-96-4
(4S)-3-<(2S,3S)-3-hydroxy-2-methyl-1-oxo-3-(1-phenylsulfanylcyclopentyl)propyl>-4-phenylmethyl-1,3-oxazolidin-2-one

: 138650-00-7
(2S,3S)-3-hydroxy-2-methyl-3-(1-phenylsulfanylcyclopentyl)propyl-N-tosylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NH₄Cl, Me₃Al, 2) BH₃ / 1) 51 - 53 deg C

2: 89 percent / DMAP

With dmap; borane; trimethylaluminum; ammonium chloride;
DOI:10.1016/0040-4039(91)80244-Z