N-benzyloxycarbonyl-homoseryl>glycine ethyl ester

Base Information

Chemical Name:N-benzyloxycarbonyl-homoseryl>glycine ethyl ester
CAS No.:126116-68-5
Molecular Formula:C₃₃H₃₈N₂O₁₀
Molecular Weight:622.672
Hs Code.:

N-benzyloxycarbonyl-<O-<(6'-hydroxy-4,4'-dimethoxydihydrochalcone)-2'-yl>homoseryl>glycine ethyl ester

Synonyms:N-benzyloxycarbonyl-homoseryl>glycine ethyl ester

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Chemical Property of N-benzyloxycarbonyl-homoseryl>glycine ethyl ester

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Technology Process of N-benzyloxycarbonyl-homoseryl>glycine ethyl ester

There total 5 articles about N-benzyloxycarbonyl-homoseryl>glycine ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.9%

: 623-33-6
glycine ethyl ester hydrochloride

: 126116-64-1
N-benzyloxycarbonyl-O-<(6'-hydroxy-4,4'-dimethoxydihydrochalcone)-2'-yl>homoserine

: 126116-68-5
N-benzyloxycarbonyl-homoseryl>glycine ethyl ester

Guidance literature:: With diethyl cyanophosphonate; triethylamine; In N,N-dimethyl-formamide; 1.) 0 deg C; 2.) RT;

Reference yield:

: 29424-96-2,102101-05-3,120851-84-5,137329-43-2,13238-06-7
naringenin-4',7-dimethyl ether

: 126116-68-5
N-benzyloxycarbonyl-homoseryl>glycine ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 86.1 percent / Et₃N, H₂ / 10percent Pd/C / ethyl acetate / 4 h / Ambient temperature

2: 60.9 percent / K₂CO₃ / dimethylformamide / 72 h / Ambient temperature

3: 92.3 percent / 4percent NaOH / acetone / 2 h / Ambient temperature

4: 97.9 percent / Et₃N, diethylphosphorocyanidate (DEPC) / dimethylformamide / 1.) 0 deg C; 2.) RT

With sodium hydroxide; diethyl cyanophosphonate; hydrogen; potassium carbonate; triethylamine; palladium on activated charcoal; In ethyl acetate; N,N-dimethyl-formamide; acetone;

Reference yield:

: 35241-54-4
2',6'-dihydroxy-4',4-dimethoxy-dihydrochalcone

: 126116-68-5
N-benzyloxycarbonyl-homoseryl>glycine ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 60.9 percent / K₂CO₃ / dimethylformamide / 72 h / Ambient temperature

2: 92.3 percent / 4percent NaOH / acetone / 2 h / Ambient temperature

3: 97.9 percent / Et₃N, diethylphosphorocyanidate (DEPC) / dimethylformamide / 1.) 0 deg C; 2.) RT

With sodium hydroxide; diethyl cyanophosphonate; potassium carbonate; triethylamine; In N,N-dimethyl-formamide; acetone;