(η-C5Me4)Fe(η-C5H4)CH2PbPh2

Base Information

Chemical Name:(η-C5Me4)Fe(η-C5H4)CH2PbPh2
CAS No.:878481-61-9
Molecular Formula:C₂₇H₂₈FePb
Molecular Weight:615.566
Hs Code.:

Synonyms:(η-C5Me4)Fe(η-C5H4)CH2PbPh2

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Chemical Property of (η-C5Me4)Fe(η-C5H4)CH2PbPh2

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Technology Process of (η-C5Me4)Fe(η-C5H4)CH2PbPh2

There total 1 articles about (η-C5Me4)Fe(η-C5H4)CH2PbPh2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (η-C5Me4CH2Li)Fe(η-C5H4Li)*0.66TMEDA

: 2117-69-3
diphenyllead(IV) dichloride

: 83928-47-6
1,2,3,4,5-pentamethyl ferrocene

: 878481-61-9
(η-C5Me4)Fe(η-C5H4)CH2PbPh2

: 3124-01-4
hexaphenyl diplumbane

Guidance literature:: In diethyl ether; byproducts: LiCl; all manipulations under N2 atm.; soln. of Pb compd. added dropwise to suspn. of Fe compd. at -78°C with stirring, stirred for 2.5 h at this temp. in dark, allowed to warm to room temp.; filtered in cold, solvent removed, by recrystallization at room temp. obtained Pb and Fe compd., purification of Fe-Pb compd. by recrystn. at -30°C proved unsuccesful;
DOI:10.1016/j.poly.2005.07.019