2-hexyl-1-octyl 6-O-(2,3,6-tri-O-benzyl-4-O-isobutyryl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Base Information

Chemical Name:2-hexyl-1-octyl 6-O-(2,3,6-tri-O-benzyl-4-O-isobutyryl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-glucopyranoside
CAS No.:1194234-41-7
Molecular Formula:C₇₂H₉₂O₁₂
Molecular Weight:1149.52
Hs Code.:

Synonyms:2-hexyl-1-octyl 6-O-(2,3,6-tri-O-benzyl-4-O-isobutyryl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

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Chemical Property of 2-hexyl-1-octyl 6-O-(2,3,6-tri-O-benzyl-4-O-isobutyryl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

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Technology Process of 2-hexyl-1-octyl 6-O-(2,3,6-tri-O-benzyl-4-O-isobutyryl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

There total 13 articles about 2-hexyl-1-octyl 6-O-(2,3,6-tri-O-benzyl-4-O-isobutyryl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1194234-40-6
2-hexyl-1-octyl 6-O-(2,3,6-tri-O-benzyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: 79-30-1
isobutyryl chloride

: 1194234-41-7
2-hexyl-1-octyl 6-O-(2,3,6-tri-O-benzyl-4-O-isobutyryl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 20h; Inert atmosphere;
DOI:10.1021/jo901569v

Reference yield:

: 1194234-31-5
octyl 4,6-O-benzylidene-β-D-thioglucopyranoside

: 1194234-41-7
2-hexyl-1-octyl 6-O-(2,3,6-tri-O-benzyl-4-O-isobutyryl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydride / N,N-dimethyl-formamide; mineral oil / Inert atmosphere

2: tetrabutylammomium bromide; silver trifluoromethanesulfonate; copper(ll) bromide / dichloromethane; acetonitrile / 0 - 20 °C / Molecular sieve; Inert atmosphere

3: hydrogenchloride; sodium cyanoborohydride / tetrahydrofuran; diethyl ether / 20 °C / Molecular sieve; Inert atmosphere

4: dmap; triethylamine / dichloromethane / 20 h / 20 °C / Inert atmosphere

With hydrogenchloride; dmap; tetrabutylammomium bromide; silver trifluoromethanesulfonate; sodium hydride; sodium cyanoborohydride; triethylamine; copper(ll) bromide; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1021/jo901569v

Reference yield:

: 1194234-32-6
octyl 2,3-di-O-benzyl-4,6-O-benzylidene-β-D-1-thioglucopyranoside

: 1194234-41-7
2-hexyl-1-octyl 6-O-(2,3,6-tri-O-benzyl-4-O-isobutyryl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutylammomium bromide; silver trifluoromethanesulfonate; copper(ll) bromide / dichloromethane; acetonitrile / 0 - 20 °C / Molecular sieve; Inert atmosphere

2: hydrogenchloride; sodium cyanoborohydride / tetrahydrofuran; diethyl ether / 20 °C / Molecular sieve; Inert atmosphere

3: dmap; triethylamine / dichloromethane / 20 h / 20 °C / Inert atmosphere

With hydrogenchloride; dmap; tetrabutylammomium bromide; silver trifluoromethanesulfonate; sodium cyanoborohydride; triethylamine; copper(ll) bromide; In tetrahydrofuran; diethyl ether; dichloromethane; acetonitrile;
DOI:10.1021/jo901569v