3-(N-cyclohexylcarbamoyl)-5-ethyl-2-imino-4,5-dimethyl-2,5-dihydrofuran

Base Information

• Chemical Name: 3-(N-cyclohexylcarbamoyl)-5-ethyl-2-imino-4,5-dimethyl-2,5-dihydrofuran
• CAS No.: 1261228-74-3
• Molecular Formula: C₁₅H₂₄N₂O₂
• Molecular Weight: 264.368

Synonyms:3-(N-cyclohexylcarbamoyl)-5-ethyl-2-imino-4,5-dimethyl-2,5-dihydrofuran

Chemical Property of 3-(N-cyclohexylcarbamoyl)-5-ethyl-2-imino-4,5-dimethyl-2,5-dihydrofuran

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Technology Process of 3-(N-cyclohexylcarbamoyl)-5-ethyl-2-imino-4,5-dimethyl-2,5-dihydrofuran

There total 2 articles about 3-(N-cyclohexylcarbamoyl)-5-ethyl-2-imino-4,5-dimethyl-2,5-dihydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

3-hydroxy-3-methyl-pentan-2-one (109916-61-2,133645-41-7,560-24-7,292611-99-5) + 2-cyano-N-cyclohexylacetamide (15029-38-6) → 3-(N-cyclohexylcarbamoyl)-5-ethyl-2-imino-4,5-dimethyl-2,5-dihydrofuran (1261228-74-3)

Guidance literature:

With sodium methylate; In methanol; at 40 ℃; for 5h;

DOI:10.1007/s11172-010-0192-2

Reference yield:

3-(N-cyclohexylcarbamoyl)-5-ethyl-2-imino-4,5-dimethyl-2,5-dihydrofuran hydrochloride (1261228-79-8) → 3-(N-cyclohexylcarbamoyl)-5-ethyl-2-imino-4,5-dimethyl-2,5-dihydrofuran (1261228-74-3)

Guidance literature:

With potassium carbonate; In water;

DOI:10.1007/s11172-010-0192-2

Reference yield: 96.0%

3-(N-cyclohexylcarbamoyl)-5-ethyl-2-imino-4,5-dimethyl-2,5-dihydrofuran (1261228-74-3) + malononitrile (109-77-3) → 3-(N-cyclohexylcarbamoyl)-2-dicyanomethylidene-5-ethyl-4,5-dimethyl-2,5-dihydrofuran (1261228-82-3)

Guidance literature:

In ethanol; at 20 ℃;

DOI:10.1007/s11172-010-0192-2

upstream raw materials:

3-(N-cyclohexylcarbamoyl)-5-ethyl-2-imino-4,5-dimethyl-2,5-dihydrofuran hydrochloride

3-hydroxy-3-methyl-pentan-2-one

2-cyano-N-cyclohexylacetamide

Downstream raw materials:

3-(N-cyclohexylcarbamoyl)-5-ethyl-2-imino-4,5-dimethyl-2,5-dihydrofuran hydrochloride

3-(N-cyclohexylcarbamoyl)-5-ethyl-4,5-dimethyl-2,5-dihydrofuran-2-one

3-(N-cyclohexylcarbamoyl)-5-ethyl-4,5-dimethyl-2-(N-methylimino)-2,5-dihydrofuran

3-(N-cyclohexylcarbamoyl)-2-dicyanomethylidene-5-ethyl-4,5-dimethyl-2,5-dihydrofuran

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