(1R,2S,5R)-5-methyl-2-[1-methyl-1-(4-nitrophenyl)ethyl]cyclohexyl acetate

Base Information

Chemical Name:(1R,2S,5R)-5-methyl-2-[1-methyl-1-(4-nitrophenyl)ethyl]cyclohexyl acetate
CAS No.:217323-75-6
Molecular Formula:C₁₈H₂₅NO₄
Molecular Weight:319.401
Hs Code.:

Synonyms:(1R,2S,5R)-5-methyl-2-[1-methyl-1-(4-nitrophenyl)ethyl]cyclohexyl acetate

Suppliers and Price of (1R,2S,5R)-5-methyl-2-[1-methyl-1-(4-nitrophenyl)ethyl]cyclohexyl acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (1R,2S,5R)-5-methyl-2-[1-methyl-1-(4-nitrophenyl)ethyl]cyclohexyl acetate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (1R,2S,5R)-5-methyl-2-[1-methyl-1-(4-nitrophenyl)ethyl]cyclohexyl acetate

There total 3 articles about (1R,2S,5R)-5-methyl-2-[1-methyl-1-(4-nitrophenyl)ethyl]cyclohexyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 200432-36-6
(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl acetate

: 217323-75-6
(1R,2S,5R)-5-methyl-2-[1-methyl-1-(4-nitrophenyl)ethyl]cyclohexyl acetate

Guidance literature:: With ammonium nitrate; trifluoroacetic anhydride; In chloroform; for 4.5h; Ambient temperature;
DOI:10.1021/jo9813078

Reference yield:

: 65253-04-5
(-)-8-phenylmenthol

: 217323-75-6
(1R,2S,5R)-5-methyl-2-[1-methyl-1-(4-nitrophenyl)ethyl]cyclohexyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / 4-(dimethylamino)pyridine, pyridine / 22 h / Ambient temperature

2: 98 percent / ammonium nitrate, trifluoroacetic anhydride / CHCl₃ / 4.5 h / Ambient temperature

With pyridine; dmap; ammonium nitrate; trifluoroacetic anhydride; In chloroform;
DOI:10.1021/jo9813078

Reference yield:

: 89-82-7,90449-51-7
pulegone

: 217323-75-6
(1R,2S,5R)-5-methyl-2-[1-methyl-1-(4-nitrophenyl)ethyl]cyclohexyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Cu₂Br₂, 2.) Na, i-PrOH

2: 95 percent / 4-(dimethylamino)pyridine, pyridine / 22 h / Ambient temperature

3: 98 percent / ammonium nitrate, trifluoroacetic anhydride / CHCl₃ / 4.5 h / Ambient temperature

With pyridine; copper(I) bromide; dmap; ammonium nitrate; sodium; isopropyl alcohol; trifluoroacetic anhydride; In chloroform;
DOI:10.1021/jo9813078