C₂₆H₂₉NO₃

Base Information

Chemical Name:C₂₆H₂₉NO₃
CAS No.:1398705-77-5
Molecular Formula:C₂₆H₂₉NO₃
Molecular Weight:403.521
Hs Code.:

C<sub>26</sub>H<sub>29</sub>NO<sub>3</sub>

Synonyms:C₂₆H₂₉NO₃

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Chemical Property of C₂₆H₂₉NO₃

Chemical Property:

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Technology Process of C₂₆H₂₉NO₃

There total 3 articles about C₂₆H₂₉NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 177947-96-5
tert-butyl 3-formylazetidine-1-carboxylate

: 1398705-77-5
C₂₆H₂₉NO₃

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 3 h / 0 °C / Inert atmosphere

2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 2 h / 0 - 20 °C

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; 1: |Grignard Reaction / 2: |Mitsunobu Displacement;
DOI:10.1021/jm3008294

Reference yield:

: 1398705-05-9
C₁₉H₂₃NO₃

: 95-48-7,77504-84-8
ortho-cresol

: 1398705-77-5
C₂₆H₂₉NO₃

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; for 2h;
DOI:10.1021/jm3008294

Reference yield:

: 142253-55-2
1-(t-butyloxycarbonyl)-azetidine-3-carboxylic acid

: 1398705-77-5
C₂₆H₂₉NO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran / 4 h / 0 °C / Inert atmosphere

2.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

2.2: 1 h / -78 °C / Inert atmosphere

3.1: tetrahydrofuran / 3 h / 0 °C / Inert atmosphere

4.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 2 h / 0 - 20 °C

With oxalyl dichloride; di-isopropyl azodicarboxylate; dimethylsulfide borane complex; dimethyl sulfoxide; triphenylphosphine; In tetrahydrofuran; dichloromethane; 2.1: |Swern Oxidation / 2.2: |Swern Oxidation / 3.1: |Grignard Reaction / 4.1: |Mitsunobu Displacement;
DOI:10.1021/jm3008294