Cs⁽¹⁺⁾*V(CN(CH₃)2C₆H₃)6^(1-)=CsV(CN(CH₃)2C₆H₃)6

Base Information

Chemical Name:Cs⁽¹⁺⁾*V(CN(CH₃)2C₆H₃)6^(1-)=CsV(CN(CH₃)2C₆H₃)6
CAS No.:200487-79-2
Molecular Formula:C₅₄H₅₄N₆V*Cs
Molecular Weight:970.91
Hs Code.:

Cs<sup>(1+)</sup>*V(CN(CH<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)6<sup>(1-)</sup>=CsV(CN(CH<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)6

Synonyms:Cs⁽¹⁺⁾*V(CN(CH₃)2C₆H₃)6^(1-)=CsV(CN(CH₃)2C₆H₃)6

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Chemical Property of Cs⁽¹⁺⁾*V(CN(CH₃)2C₆H₃)6^(1-)=CsV(CN(CH₃)2C₆H₃)6

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Technology Process of Cs⁽¹⁺⁾*V(CN(CH₃)2C₆H₃)6^(1-)=CsV(CN(CH₃)2C₆H₃)6

There total 2 articles about Cs⁽¹⁺⁾*V(CN(CH₃)2C₆H₃)6^(1-)=CsV(CN(CH₃)2C₆H₃)6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: cesium graphite

: 200487-82-7
V(CN(CH₃)2C₆H₃)6

: 200487-79-2
Cs⁽¹⁺⁾*V(CN(CH₃)2C₆H₃)6^(1-)=CsV(CN(CH₃)2C₆H₃)6

Guidance literature:: In tetrahydrofuran; -50°C; recrystn. (THF/heptane); elem. anal.;
DOI:10.1021/ja9729239

Reference yield:

: 119072-54-7,2769-71-3
2,6-dimethylphenyl isonitrile

: 200487-79-2
Cs⁽¹⁺⁾*V(CN(CH₃)2C₆H₃)6^(1-)=CsV(CN(CH₃)2C₆H₃)6

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran; n-heptane

2: tetrahydrofuran

In tetrahydrofuran; n-heptane;
DOI:10.1021/ja9729239

Reference yield: 87.0%

: 17455-13-9
18-crown-6 ether

: 200487-79-2
Cs⁽¹⁺⁾*V(CN(CH₃)2C₆H₃)6^(1-)=CsV(CN(CH₃)2C₆H₃)6

: Cs⁽¹⁺⁾*2(CH₂)12O₆*V(CN(CH₃)2C₆H₃)6^(1-)=Cs((CH₂)12O₆)2V(CN(CH₃)2C₆H₃)6

Guidance literature:: In tetrahydrofuran; ligand in THF at -60°C was transferred into flask with V-complex in THF at -60°C, stirred for 15 h, warmed to room temp. under Ar; filtered, heptane was added, solvent was removed in vacuo, filtered off,washed with pentane, dried under vac., recrystd. from THF/pentane, drie d in vacuo for 18 h; elem. anal.;
DOI:10.1021/ja000212w