[1-(15)N]-6-benzyloxy-2-chloro-9-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)purine

Base Information

• Chemical Name: [1-(15)N]-6-benzyloxy-2-chloro-9-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)purine
• CAS No.: 1234319-78-8
• Molecular Formula: C₂₃H₂₃ClN₄O₈
• Molecular Weight: 519.904

Synonyms:[1-(15)N]-6-benzyloxy-2-chloro-9-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)purine

Chemical Property of [1-(15)N]-6-benzyloxy-2-chloro-9-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)purine

Chemical Property:

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Technology Process of [1-(15)N]-6-benzyloxy-2-chloro-9-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)purine

There total 1 articles about [1-(15)N]-6-benzyloxy-2-chloro-9-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

[1-(15)N]-2,6-dichloro-9-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)purine (1234319-75-5) + benzyl alcohol (100-51-6,185532-71-2) → [1-(15)N]-6-benzyloxy-2-chloro-9-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)purine (1234319-78-8)

Guidance literature:

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In toluene; at 80 ℃; Inert atmosphere;

DOI:10.1021/jo100808w

Reference yield:

ISOPROPYLAMIDE (563-83-7) + [1-(15)N]-6-benzyloxy-2-chloro-9-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)purine (1234319-78-8) → [1-(15)N]-2',3',5'-tri-O-acetyl-6-O-benzyl-2-N-isobutyrylguanosine (1234319-96-0)

Guidance literature:

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In toluene; at 110 ℃; Inert atmosphere;

DOI:10.1021/jo100808w

Reference yield:

[(15)N]isobutyramide (62962-45-2) + [1-(15)N]-6-benzyloxy-2-chloro-9-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)purine (1234319-78-8) → [1-(15)N,2-(15)NH2]-2',3',5'-tri-O-acetyl-6-O-benzyl-2-N-isobutyrylguanosine (1234319-98-2)

Guidance literature:

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; In toluene; at 110 ℃; Inert atmosphere;

DOI:10.1021/jo100808w

upstream raw materials:

[1-(15)N]-2,6-dichloro-9-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)purine

benzyl alcohol

Downstream raw materials:

[1-⁽¹⁵⁾N]-2',3',5'-tri-O-acetyl-6-O-benzyl-2-N-isobutyrylguanosine

[1-⁽¹⁵⁾N,2-⁽¹⁵⁾NH₂]-2',3',5'-tri-O-acetyl-6-O-benzyl-2-N-isobutyrylguanosine

[1-⁽¹⁵⁾N,2-⁽¹⁵⁾NH₂]-2',3',5'-tri-O-acetyl-2-N-benzoyl-6-O-benzylguanosine

[1-⁽¹⁵⁾N]-2',3',5'-tri-O-acetyl-2-N-benzoyl-6-O-benzylguanosine

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