1-(3,4-dihydroxyphenyl)-2-[3-(3,4-dihydroxyphenyl)-4,6-dimethoxy-1H-indol-1-yl]ethanone

Base Information

• Chemical Name: 1-(3,4-dihydroxyphenyl)-2-[3-(3,4-dihydroxyphenyl)-4,6-dimethoxy-1H-indol-1-yl]ethanone
• CAS No.: 1609489-59-9
• Molecular Formula: C₂₄H₂₁NO₇
• Molecular Weight: 435.433

Synonyms:1-(3,4-dihydroxyphenyl)-2-[3-(3,4-dihydroxyphenyl)-4,6-dimethoxy-1H-indol-1-yl]ethanone

Chemical Property of 1-(3,4-dihydroxyphenyl)-2-[3-(3,4-dihydroxyphenyl)-4,6-dimethoxy-1H-indol-1-yl]ethanone

Chemical Property:

Purity/Quality:

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Technology Process of 1-(3,4-dihydroxyphenyl)-2-[3-(3,4-dihydroxyphenyl)-4,6-dimethoxy-1H-indol-1-yl]ethanone

There total 2 articles about 1-(3,4-dihydroxyphenyl)-2-[3-(3,4-dihydroxyphenyl)-4,6-dimethoxy-1H-indol-1-yl]ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-bromo-1-(3,4-dihydroxyphenyl)ethanone (40131-99-5) + 3.5-dimethoxyaniline (10272-07-8) → 1-(3,4-dihydroxyphenyl)-2-[3-(3,4-dihydroxyphenyl)-4,6-dimethoxy-1H-indol-1-yl]ethanone (1609489-59-9)

Guidance literature:

With sodium hydrogencarbonate; In ethanol; for 16h; Reflux;

Reference yield:

→ 1-(3,4-dihydroxyphenyl)-2-[3-(3,4-dihydroxyphenyl)-4,6-dimethoxy-1H-indol-1-yl]ethanone (1609489-59-9)

Guidance literature:

With N,N-dimethyl-aniline; In 5,5-dimethyl-1,3-cyclohexadiene; for 24h; Reflux;

Reference yield:

1-(3,4-dihydroxyphenyl)-2-[3-(3,4-dihydroxyphenyl)-4,6-dimethoxy-1H-indol-1-yl]ethanone (1609489-59-9) + acetic anhydride (108-24-7) → 4-{1-[2-(3,4-diacetoxyphenyl)-2-oxoethyl]-4,6-dimethoxy-1H-indol-3-yl}-1,2-phenylene diacetate (1609489-81-7)

Guidance literature:

With pyridine; at 0 - 20 ℃; for 16h; Inert atmosphere;

upstream raw materials:

2-bromo-1-(3,4-dihydroxyphenyl)ethanone

3.5-dimethoxyaniline

Downstream raw materials:

4-{1-[2-(3,4-diacetoxyphenyl)-2-oxoethyl]-4,6-dimethoxy-1H-indol-3-yl}-1,2-phenylene diacetate

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