Cyclopentanecarboxylic acid, 2-amino-3-methyl-, 1,1-dimethylethyl ester, (1S,2R,3S)- (9CI)

Base Information

Chemical Name:Cyclopentanecarboxylic acid, 2-amino-3-methyl-, 1,1-dimethylethyl ester, (1S,2R,3S)- (9CI)
CAS No.:816444-35-6
Molecular Formula:C₁₁H₂₁NO₂
Molecular Weight:199.293
Hs Code.:
Mol file:816444-35-6.mol

Synonyms:Cyclopentanecarboxylic acid, 2-amino-3-methyl-, 1,1-dimethylethyl ester, (1S,2R,3S)- (9CI)

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Chemical Property of Cyclopentanecarboxylic acid, 2-amino-3-methyl-, 1,1-dimethylethyl ester, (1S,2R,3S)- (9CI)

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Technology Process of Cyclopentanecarboxylic acid, 2-amino-3-methyl-, 1,1-dimethylethyl ester, (1S,2R,3S)- (9CI)

There total 10 articles about Cyclopentanecarboxylic acid, 2-amino-3-methyl-, 1,1-dimethylethyl ester, (1S,2R,3S)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 479201-51-9
tert-butyl (1S,2S,3R,αS)-3-methyl-2-(N-benzyl-N-α-methylbenzylamino)cyclopentane-1-carboxylate

: 646518-16-3,816444-35-6
tert-butyl (1S,2S,3R)-3-methyl-2-aminocyclopentane-1-carboxylate

Guidance literature:: With 20 % Pd(OH)2/C; hydrogen; In methanol; at 20 ℃; for 16h; under 3800.26 Torr;
DOI:10.1016/j.tetasy.2010.12.007

Reference yield: 82.0%

: tert-butyl (1S,2R,3S,αR)-3-methyl-2-(N-α-methylbenzylamino)cyclopentane-1-carboxylate

: 816444-35-6
tert-butyl (1S,2R,3S)-3-methyl-2-aminocyclopentane-1-carboxylate

Guidance literature:: tert-butyl (1S,2R,3S,αR)-3-methyl-2-(N-α-methylbenzylamino)cyclopentane-1-carboxylate; With 20 % Pd(OH)2/C; hydrogen; acetic acid; In methanol; for 36h; under 3800.26 Torr;

With sodium hydrogencarbonate; In dichloromethane; water;
DOI:10.1007/s10870-011-0164-x