(E)-4-(2,3,5-Tri-O-benzoyl-β-D-ribofuranosyl)-1-ethoxymethylenesemicarbazide

Base Information

• Chemical Name: (E)-4-(2,3,5-Tri-O-benzoyl-β-D-ribofuranosyl)-1-ethoxymethylenesemicarbazide
• CAS No.: 98292-39-8
• Molecular Formula: C₃₀H₂₉N₃O₉
• Molecular Weight: 575.575

Synonyms:(E)-4-(2,3,5-Tri-O-benzoyl-β-D-ribofuranosyl)-1-ethoxymethylenesemicarbazide

Chemical Property of (E)-4-(2,3,5-Tri-O-benzoyl-β-D-ribofuranosyl)-1-ethoxymethylenesemicarbazide

Chemical Property:

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Technology Process of (E)-4-(2,3,5-Tri-O-benzoyl-β-D-ribofuranosyl)-1-ethoxymethylenesemicarbazide

There total 1 articles about (E)-4-(2,3,5-Tri-O-benzoyl-β-D-ribofuranosyl)-1-ethoxymethylenesemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

4-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)semicarbazide (71397-61-0) + orthoformic acid triethyl ester (122-51-0) → (E)-4-(2,3,5-Tri-O-benzoyl-β-D-ribofuranosyl)-1-ethoxymethylenesemicarbazide (98292-39-8)

Guidance literature:

With formic acid; In dichloromethane; for 4h; Ambient temperature;

Reference yield: 53.0%

(E)-4-(2,3,5-Tri-O-benzoyl-β-D-ribofuranosyl)-1-ethoxymethylenesemicarbazide (98292-39-8) → 4-(2,3,5-Tri-O-benzoyl-β-D-ribofuranosyl)-1,2,4-triazol-3(2H)-one (80049-44-1)

Guidance literature:

With ammonium sulfate; 1,1,1,3,3,3-hexamethyl-disilazane; In xylene; for 10h; Heating;

upstream raw materials:

4-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)semicarbazide

orthoformic acid triethyl ester

Downstream raw materials:

4-(2,3,5-Tri-O-benzoyl-β-D-ribofuranosyl)-1,2,4-triazol-3(2H)-one

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