[(C₅H₅)(CO)2Fe(N₄CC₆H₄CN)]

Base Information

Chemical Name:[(C₅H₅)(CO)2Fe(N₄CC₆H₄CN)]
CAS No.:463945-92-8
Molecular Formula:C₁₅H₉FeN₅O₂
Molecular Weight:347.116
Hs Code.:

[(C<sub>5</sub>H<sub>5</sub>)(CO)2Fe(N<sub>4</sub>CC<sub>6</sub>H<sub>4</sub>CN)]

Synonyms:[(C₅H₅)(CO)2Fe(N₄CC₆H₄CN)]

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Chemical Property of [(C₅H₅)(CO)2Fe(N₄CC₆H₄CN)]

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Technology Process of [(C₅H₅)(CO)2Fe(N₄CC₆H₄CN)]

There total 3 articles about [(C₅H₅)(CO)2Fe(N₄CC₆H₄CN)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: C₅H₅Fe(CO)2(HN₄CC₆H₄CN)⁽¹⁺⁾*CF₃O₂SO^(1-)=[C₅H₅Fe(CO)2(HN₄CC₆H₄CN)](CF₃O₂SO)

: 463945-92-8
[(C₅H₅)(CO)2Fe(N₄CC₆H₄CN)]

Guidance literature:: With base; In acetonitrile; Ar; addn. of stoich. amt. of base to acetonitrile soln. of the complex;
DOI:10.1021/om020283z

Reference yield: 76.0%

: sodium azide

: 463945-77-9
[(cyclopentadienyl)Fe(CO)2(1,4-dicyanobenzene)](CF₃SO₃)

: 463945-92-8
[(C₅H₅)(CO)2Fe(N₄CC₆H₄CN)]

Guidance literature:: In dichloromethane; byproducts: Fe2(C5H5)2(CO)4; Ar; addn. of slight excess of sodium azide to a dichloromethane soln. ofthe complex, stirring the suspn. at room temp. for 10 h; filtering on Celite, evapn. to dryness, chromy. of the residue on Al2O3 with CH2Cl2, further with CH2Cl2-CH3CN (2:1 vol.); elem anal.;
DOI:10.1021/om020283z

Reference yield:

: 14389-10-7
5-(4-cyanophenyl)tetrazole

: 152572-89-9
[Fe(CO)2(tetrahydrofuran)(Cp)]SO₃CF₃

: 463945-92-8
[(C₅H₅)(CO)2Fe(N₄CC₆H₄CN)]

: 852834-73-2
[(C₅H₅)(CO)2Fe(N₄CC₆H₄CN)Fe(CO)2(C₅H₅)]⁽¹⁺⁾*O₃SCF₃^(1-)=[(C₅H₅)(CO)2Fe(N₄CC₆H₄CN)Fe(CO)2(C₅H₅)](O₃SCF₃)

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; (Ar); Schlenk technique; suspn. of tetrazole in DMF was treated with Et3N; soln. was added to soln. of Fe complex in DMF; mixt. was reacted for 4 h; IR monitoring; evapd.; dissolved in CH2Cl2; filtered; chromd. (alumina, CH2Cl2/CH3CN);
DOI:10.1016/j.jorganchem.2004.12.007