p-methoxyphenyl 2,3-di-O-acetyl-4-O-trichloroethylsulfo-6-O-benzyl-β-D-glucopyranoside

Base Information

• Chemical Name: p-methoxyphenyl 2,3-di-O-acetyl-4-O-trichloroethylsulfo-6-O-benzyl-β-D-glucopyranoside
• CAS No.: 1185733-79-2
• Molecular Formula: C₂₆H₂₉Cl₃O₁₂S
• Molecular Weight: 671.934

Synonyms:p-methoxyphenyl 2,3-di-O-acetyl-4-O-trichloroethylsulfo-6-O-benzyl-β-D-glucopyranoside

Chemical Property of p-methoxyphenyl 2,3-di-O-acetyl-4-O-trichloroethylsulfo-6-O-benzyl-β-D-glucopyranoside

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Technology Process of p-methoxyphenyl 2,3-di-O-acetyl-4-O-trichloroethylsulfo-6-O-benzyl-β-D-glucopyranoside

There total 6 articles about p-methoxyphenyl 2,3-di-O-acetyl-4-O-trichloroethylsulfo-6-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

p-methoxyphenyl 2,3-di-O-acetyl-6-O-benzyl-β-D-glucopyranoside (1009006-57-8) + 2,2,2-trichloroethoxysulfuryl 2-methyl-3-methylimidazolium triflate (1185733-70-3) → p-methoxyphenyl 2,3-di-O-acetyl-4-O-trichloroethylsulfo-6-O-benzyl-β-D-glucopyranoside (1185733-79-2)

Guidance literature:

With 1,2-dimethyl-1H-imidazole; In dichloromethane; at 0 - 20 ℃; for 24h; Inert atmosphere;

DOI:10.1021/jo9014112

Reference yield: 79.0%

p-methoxyphenyl 2,3-di-O-acetyl-6-O-benzyl-β-D-glucopyranoside (1009006-57-8) + 2,3-dimethyl-1-((2,2,2-trichloroethoxy)-sulfonyl)-1H-imidazol-3-ium tetrafluoroborate → p-methoxyphenyl 2,3-di-O-acetyl-4-O-trichloroethylsulfo-6-O-benzyl-β-D-glucopyranoside (1185733-79-2)

Guidance literature:

With 1,2-dimethyl-1H-imidazole; In dichloromethane; at 0 - 20 ℃; for 20h; Inert atmosphere;

DOI:10.1021/jo9014112

Reference yield: 78.0%

p-methoxyphenyl 2,3-di-O-acetyl-6-O-benzyl-β-D-glucopyranoside (1009006-57-8) + 1-(2,2,2-trichloroethoxysulfuryl)-2-ethyl-3-methylimidazolium tetrafluoroborate → p-methoxyphenyl 2,3-di-O-acetyl-4-O-trichloroethylsulfo-6-O-benzyl-β-D-glucopyranoside (1185733-79-2)

Guidance literature:

With 1,2-dimethyl-1H-imidazole; In dichloromethane; at 0 - 20 ℃; for 20h; Inert atmosphere;

DOI:10.1021/jo9014112

upstream raw materials:

p-methoxyphenyl 2,3-di-O-acetyl-6-O-benzyl-β-D-glucopyranoside

2,2,2-trichloroethoxysulfuryl 2-methyl-3-methylimidazolium triflate

1-(2,2,2-trichloroethoxysulfuryl)-2-ethyl-3-methylimidazolium triflate

1-(2,2,2-trichloroethoxysulfuryl)-2-isopropyl-3-methylimidazolium triflate

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