methyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1→3)-[(2,3,4,6,7-penta-O-benzyl-L-glycero-α-D-manno-heptopyranosyl)-(1→7)]-2-O-benzoyl-4-O-dibenzyloxyphosphoryl-6-O-(3-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-1-yl)-L-glycero-α-D-mannoheptopyranoside

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Chemical Name:methyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1→3)-[(2,3,4,6,7-penta-O-benzyl-L-glycero-α-D-manno-heptopyranosyl)-(1→7)]-2-O-benzoyl-4-O-dibenzyloxyphosphoryl-6-O-(3-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-1-yl)-L-glycero-α-D-mannoheptopyranoside
CAS No.:1520094-98-7
Molecular Formula:C₁₁₇H₁₃₆FO₂₃PSi₂
Molecular Weight:2016.5
Hs Code.:

methyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1→3)-[(2,3,4,6,7-penta-O-benzyl-L-glycero-α-D-manno-heptopyranosyl)-(1→7)]-2-O-benzoyl-4-O-dibenzyloxyphosphoryl-6-O-(3-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-1-yl)-L-glycero-α-D-mannoheptopyranoside

Synonyms:methyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1→3)-[(2,3,4,6,7-penta-O-benzyl-L-glycero-α-D-manno-heptopyranosyl)-(1→7)]-2-O-benzoyl-4-O-dibenzyloxyphosphoryl-6-O-(3-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-1-yl)-L-glycero-α-D-mannoheptopyranoside

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Chemical Property of methyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1→3)-[(2,3,4,6,7-penta-O-benzyl-L-glycero-α-D-manno-heptopyranosyl)-(1→7)]-2-O-benzoyl-4-O-dibenzyloxyphosphoryl-6-O-(3-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-1-yl)-L-glycero-α-D-mannoheptopyranoside

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Technology Process of methyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1→3)-[(2,3,4,6,7-penta-O-benzyl-L-glycero-α-D-manno-heptopyranosyl)-(1→7)]-2-O-benzoyl-4-O-dibenzyloxyphosphoryl-6-O-(3-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-1-yl)-L-glycero-α-D-mannoheptopyranoside

There total 1 articles about methyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1→3)-[(2,3,4,6,7-penta-O-benzyl-L-glycero-α-D-manno-heptopyranosyl)-(1→7)]-2-O-benzoyl-4-O-dibenzyloxyphosphoryl-6-O-(3-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-1-yl)-L-glycero-α-D-mannoheptopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.5%

: 1520094-93-2
methyl (2,3,4,6,7-penta-O-benzyl-L-glycero-α-D-manno-heptopyranosyl)-(1→7)-2-O-benzoyl-4-O-dibenzyloxyphosphoryl-6-O-(3-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-1-yl)-L-glycero-α-D-manno-heptopyranoside

: 339276-14-1
2,3,4,6-tetra-O-benzyl-D-glucopyranosyl 1-(N-phenyl)-2,2,2-trifluoroacetimidate

: 1520094-98-7
methyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1→3)-[(2,3,4,6,7-penta-O-benzyl-L-glycero-α-D-manno-heptopyranosyl)-(1→7)]-2-O-benzoyl-4-O-dibenzyloxyphosphoryl-6-O-(3-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-1-yl)-L-glycero-α-D-mannoheptopyranoside

: 1520095-17-3
methyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1→3)-[(2,3,4,6,7-penta-O-benzyl-L-glycero-β-D-manno-heptopyranosyl)-(1→7)]-2-O-benzoyl-4-O-dibenzyloxyphosphoryl-6-O-(3-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-1-yl)-L-glycero-α-D-mannoheptopyranoside

Guidance literature:: With t-butyldimethylsiyl triflate; In dichloromethane; toluene; at -22 ℃; for 2h; Inert atmosphere; Molecular sieve;
DOI:10.1021/jo402312x