4-aminophenoxyethyl tetrahydro-2H-pyran-2-yl ether

Base Information

Chemical Name:4-aminophenoxyethyl tetrahydro-2H-pyran-2-yl ether
CAS No.:445283-42-1
Molecular Formula:C₁₃H₁₉NO₃
Molecular Weight:237.299
Hs Code.:

Synonyms:4-aminophenoxyethyl tetrahydro-2H-pyran-2-yl ether

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Chemical Property of 4-aminophenoxyethyl tetrahydro-2H-pyran-2-yl ether

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Technology Process of 4-aminophenoxyethyl tetrahydro-2H-pyran-2-yl ether

There total 2 articles about 4-aminophenoxyethyl tetrahydro-2H-pyran-2-yl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 445283-41-0
4-nitrophenoxyethyl tetrahydro-2H-pyran-2-yl ether

: 445283-42-1
4-aminophenoxyethyl tetrahydro-2H-pyran-2-yl ether

Guidance literature:: With hydrogen; 5percentPd/C; In ethyl acetate; at 20 ℃; for 4h; under 2280.15 Torr;
DOI:10.1021/jm0201518

Reference yield:

: 17739-45-6,59146-56-4
2-(2-bromoethoxy)tetrahydropyran

: 445283-42-1
4-aminophenoxyethyl tetrahydro-2H-pyran-2-yl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: KOH / dimethylsulfoxide / 0.08 h / 20 °C

1.2: 21 percent / dimethylsulfoxide / 16 h / 20 °C

2.1: 100 percent / H₂ / 5percentPd/C / ethyl acetate / 4 h / 20 °C / 2280.15 Torr

With potassium hydroxide; hydrogen; 5percentPd/C; In dimethyl sulfoxide; ethyl acetate;
DOI:10.1021/jm0201518