Benzenesulfinamide, N-(2E)-2-butenylidene-4-methyl-, [N(E)]- (9CI)

Base Information

Chemical Name:Benzenesulfinamide, N-(2E)-2-butenylidene-4-methyl-, [N(E)]- (9CI)
CAS No.:813461-58-4
Molecular Formula:C₁₁H₁₃NOS
Molecular Weight:207.296
Hs Code.:
Mol file:813461-58-4.mol

Synonyms:Benzenesulfinamide,N-(2E)-2-butenylidene-4-methyl-, [N(E)]- (9CI)

Suppliers and Price of Benzenesulfinamide, N-(2E)-2-butenylidene-4-methyl-, [N(E)]- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Benzenesulfinamide, N-(2E)-2-butenylidene-4-methyl-, [N(E)]- (9CI)

Chemical Property:

Purity/Quality:

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Technology Process of Benzenesulfinamide, N-(2E)-2-butenylidene-4-methyl-, [N(E)]- (9CI)

There total 8 articles about Benzenesulfinamide, N-(2E)-2-butenylidene-4-methyl-, [N(E)]- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 123-73-9,4170-30-3
trans-Crotonaldehyde

: 188447-91-8
(S)-p-toluenesulfinimide

: 188447-82-7,813461-58-4
(S)-(+)-N-(crotonylidene)-p-toluenesulfinamide

Guidance literature:: With titanium(IV) tetraethanolate; In dichloromethane; at 20 - 50 ℃; for 4.5h;

Reference yield: 76.0%

: 123-73-9,4170-30-3
trans-Crotonaldehyde

: 6873-55-8
p-tolylsulfinyl amide

: 813461-58-4
C₇H₇SONCHC₃H₅

Guidance literature:: With potassium tert-butylate; In methanol; at 20 ℃; for 16h;
DOI:10.1016/j.tetasy.2007.10.015

Reference yield: 60.0%

: 123-73-9,4170-30-3
trans-Crotonaldehyde

: 1517-82-4
(-)-menthyl p-toluenesulfinate

: 188447-82-7,813461-58-4
(S)-(+)-N-(crotonylidene)-p-toluenesulfinamide

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 - 20 ℃; Product distribution; effect of the presence of KF;
DOI:10.1021/jo970077e