7-Quinolinecarboxylicacid,1,2-dihydro-3-methyl-2-oxo-,methylester(9CI)

Base Information

Chemical Name:7-Quinolinecarboxylicacid,1,2-dihydro-3-methyl-2-oxo-,methylester(9CI)
CAS No.:813425-28-4
Molecular Formula:C₁₂H₁₁NO₃
Molecular Weight:217.224
Hs Code.:
Mol file:813425-28-4.mol

Synonyms:7-Quinolinecarboxylicacid,1,2-dihydro-3-methyl-2-oxo-,methylester(9CI)

Suppliers and Price of 7-Quinolinecarboxylicacid,1,2-dihydro-3-methyl-2-oxo-,methylester(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-Quinolinecarboxylicacid,1,2-dihydro-3-methyl-2-oxo-,methylester(9CI)

Chemical Property:

PSA：59.16000
LogP:1.62310

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 7-Quinolinecarboxylicacid,1,2-dihydro-3-methyl-2-oxo-,methylester(9CI)

There total 3 articles about 7-Quinolinecarboxylicacid,1,2-dihydro-3-methyl-2-oxo-,methylester(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: methyl 4-formyl-3-propionamidobenzoate

: 813425-28-4
methyl 3-methyl-2-oxo-1,2-dihydroquinoline-7-carboxylate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 2h; Inert atmosphere;

Reference yield:

: 813425-67-1
Methyl 3-amino-4-(1-hydroxy-3-methoxy-2-methyl-3-oxopropyl)benzoate

: 813425-28-4
methyl 3-methyl-2-oxo-1,2-dihydroquinoline-7-carboxylate

Guidance literature:: With hydrogenchloride; In 1,4-dioxane;

Reference yield:

: 90484-53-0
3-bromo-4-formyl-benzoic acid methyl ester

: 813425-28-4
methyl 3-methyl-2-oxo-1,2-dihydroquinoline-7-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 12 h / 75 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 2 h / 100 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium carbonate; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In N,N-dimethyl-formamide;