methyl 3-(5-(2-(methoxycarbonyloxy)ethyl)-2-phenylbenzo[b]furan-7-yl)benzoate

Base Information

Chemical Name:methyl 3-(5-(2-(methoxycarbonyloxy)ethyl)-2-phenylbenzo[b]furan-7-yl)benzoate
CAS No.:1422250-76-7
Molecular Formula:C₂₆H₂₂O₆
Molecular Weight:430.457
Hs Code.:

Synonyms:methyl 3-(5-(2-(methoxycarbonyloxy)ethyl)-2-phenylbenzo[b]furan-7-yl)benzoate

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Chemical Property of methyl 3-(5-(2-(methoxycarbonyloxy)ethyl)-2-phenylbenzo[b]furan-7-yl)benzoate

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Technology Process of methyl 3-(5-(2-(methoxycarbonyloxy)ethyl)-2-phenylbenzo[b]furan-7-yl)benzoate

There total 4 articles about methyl 3-(5-(2-(methoxycarbonyloxy)ethyl)-2-phenylbenzo[b]furan-7-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1422250-63-2
C₁₈H₁₅ClO₄

: 99769-19-4
[3-(methoxycarbonyl)phenyl]boronic acid

: 1422250-76-7
methyl 3-(5-(2-(methoxycarbonyloxy)ethyl)-2-phenylbenzo[b]furan-7-yl)benzoate

Guidance literature:: With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In 1,4-dioxane; at 100 ℃; for 3h;
DOI:10.1016/j.tet.2012.12.058

Reference yield:

: 1422251-06-6
3-chloro-4-hydroxyphenethyl methyl carbonate

: 1422250-76-7
methyl 3-(5-(2-(methoxycarbonyloxy)ethyl)-2-phenylbenzo[b]furan-7-yl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: iodine; silver sulfate / ethanol / 20 °C

2: potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / 1,4-dioxane / 110 °C

3: potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / 1,4-dioxane / 3 h / 100 °C

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; iodine; silver sulfate; In 1,4-dioxane; ethanol; 3: |Suzuki-Miyaura Coupling;
DOI:10.1016/j.tet.2012.12.058

Reference yield:

: 1422251-05-5
3-chloro-4-hydroxy-5-iodophenethyl methyl carbonate

: 1422250-76-7
methyl 3-(5-(2-(methoxycarbonyloxy)ethyl)-2-phenylbenzo[b]furan-7-yl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / 1,4-dioxane / 110 °C

2: potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / 1,4-dioxane / 3 h / 100 °C

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In 1,4-dioxane; 2: |Suzuki-Miyaura Coupling;
DOI:10.1016/j.tet.2012.12.058