C₃₄H₄₅N₅O₉

Base Information

Chemical Name:C₃₄H₄₅N₅O₉
CAS No.:1438408-32-2
Molecular Formula:C₃₄H₄₅N₅O₉
Molecular Weight:667.759
Hs Code.:

C<sub>34</sub>H<sub>45</sub>N<sub>5</sub>O<sub>9</sub>

Synonyms:C₃₄H₄₅N₅O₉

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Chemical Property of C₃₄H₄₅N₅O₉

Chemical Property:

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Technology Process of C₃₄H₄₅N₅O₉

There total 11 articles about C₃₄H₄₅N₅O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1438408-31-1
C₃₄H₄₄N₂O₉

: 1438408-32-2
C₃₄H₄₅N₅O₉

Guidance literature:: C₃₄H₄₄N₂O₉; With Trimethyl borate; In N,N-dimethyl-formamide; at 20 ℃; for 0.333333h; Inert atmosphere;

With sodium azide; In N,N-dimethyl-formamide; at 50 ℃; for 3h; regioselective reaction; Inert atmosphere;
DOI:10.1039/c3cc42365d

Reference yield:

: 1438408-16-2
C₁₄H₂₅NO₄

: 1438408-32-2
C₃₄H₄₅N₅O₉

Guidance literature:: Multi-step reaction with 9 steps

1.1: 1H-imidazole; triphenylphosphine; iodine / dichloromethane / 2 h / Cooling with ice; Inert atmosphere

2.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / Cooling with ice; Inert atmosphere

2.2: 8 h / 20 °C / Inert atmosphere

2.3: 3.33 h / 20 °C / Inert atmosphere

3.1: C₁₅H₂₆Cl₂CuN₂O₂; triethylamine / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

4.1: Dess-Martin periodane / dichloromethane / 5 h / Cooling with ice; Inert atmosphere

5.1: dichloromethane / 15 h / 50 °C / Inert atmosphere

6.1: sodium hydrogencarbonate; mercuric triflate / dichloromethane / 10.5 h / -20 °C / Inert atmosphere; Cooling with ice

6.2: 0.5 h / -78 °C / Inert atmosphere

7.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 1 h / -78 °C / Inert atmosphere

8.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 10.33 h / -40 - -20 °C / Inert atmosphere

9.1: Trimethyl borate / N,N-dimethyl-formamide / 0.33 h / 20 °C / Inert atmosphere

9.2: 3 h / 50 °C / Inert atmosphere

With 1H-imidazole; Trimethyl borate; C₁₅H₂₆Cl₂CuN₂O₂; iodine; mercuric triflate; diisobutylaluminium hydride; sodium hydrogencarbonate; caesium carbonate; Dess-Martin periodane; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; 4.1: |Dess-Martin Oxidation / 5.1: |Wittig Olefination;
DOI:10.1039/c3cc42365d

Reference yield:

: 1438408-17-3
C₁₄H₂₄INO₃

: 1438408-32-2
C₃₄H₄₅N₅O₉

Guidance literature:: Multi-step reaction with 8 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / Cooling with ice; Inert atmosphere

1.2: 8 h / 20 °C / Inert atmosphere

1.3: 3.33 h / 20 °C / Inert atmosphere

2.1: C₁₅H₂₆Cl₂CuN₂O₂; triethylamine / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

3.1: Dess-Martin periodane / dichloromethane / 5 h / Cooling with ice; Inert atmosphere

4.1: dichloromethane / 15 h / 50 °C / Inert atmosphere

5.1: sodium hydrogencarbonate; mercuric triflate / dichloromethane / 10.5 h / -20 °C / Inert atmosphere; Cooling with ice

5.2: 0.5 h / -78 °C / Inert atmosphere

6.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 1 h / -78 °C / Inert atmosphere

7.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 10.33 h / -40 - -20 °C / Inert atmosphere

8.1: Trimethyl borate / N,N-dimethyl-formamide / 0.33 h / 20 °C / Inert atmosphere

8.2: 3 h / 50 °C / Inert atmosphere

With Trimethyl borate; C₁₅H₂₆Cl₂CuN₂O₂; mercuric triflate; diisobutylaluminium hydride; sodium hydrogencarbonate; caesium carbonate; Dess-Martin periodane; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; 3.1: |Dess-Martin Oxidation / 4.1: |Wittig Olefination;
DOI:10.1039/c3cc42365d