1,13-Dimethyl-3,11,15,23,26,34-hexaoxa-6,20,29-trioxo-7,19,30-trisbenzyloxyazabicyclo<11,11,11>pentatriacontane

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Chemical Name:1,13-Dimethyl-3,11,15,23,26,34-hexaoxa-6,20,29-trioxo-7,19,30-trisbenzyloxyazabicyclo<11,11,11>pentatriacontane
CAS No.:123074-28-2
Molecular Formula:C₄₉H₆₉N₃O₁₂
Molecular Weight:892.1
Hs Code.:

Synonyms:1,13-Dimethyl-3,11,15,23,26,34-hexaoxa-6,20,29-trioxo-7,19,30-trisbenzyloxyazabicyclo<11,11,11>pentatriacontane

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Chemical Property of 1,13-Dimethyl-3,11,15,23,26,34-hexaoxa-6,20,29-trioxo-7,19,30-trisbenzyloxyazabicyclo<11,11,11>pentatriacontane

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Technology Process of 1,13-Dimethyl-3,11,15,23,26,34-hexaoxa-6,20,29-trioxo-7,19,30-trisbenzyloxyazabicyclo<11,11,11>pentatriacontane

There total 7 articles about 1,13-Dimethyl-3,11,15,23,26,34-hexaoxa-6,20,29-trioxo-7,19,30-trisbenzyloxyazabicyclo<11,11,11>pentatriacontane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 123074-24-8
1,1,1-Tris(chlorocarbonylethoxymethyl)ethane

: 123074-27-1
1,1,1-Tris(O-benzylhydroxylaminopropoxymethyl)ethane

: 123074-28-2
1,13-Dimethyl-3,11,15,23,26,34-hexaoxa-6,20,29-trioxo-7,19,30-trisbenzyloxyazabicyclo<11,11,11>pentatriacontane

Guidance literature:: With pyridine; In benzene; for 12h; Ambient temperature;
DOI:10.1016/S0040-4020(01)88367-8

Reference yield:

: 77-85-0
2-(hydroxymethyl)-2-methylpropane-1,3-diol

: 123074-28-2
1,13-Dimethyl-3,11,15,23,26,34-hexaoxa-6,20,29-trioxo-7,19,30-trisbenzyloxyazabicyclo<11,11,11>pentatriacontane

Guidance literature:: Multi-step reaction with 6 steps

1: 83 percent / dioxane / 25 - 35 °C / cyanoethylation

2: 64 percent / HCl (g)

3: 83 percent / LiAlH₄

5: 1,2-dimethoxy-ethane

6: 30 percent / benzene

With hydrogenchloride; lithium aluminium tetrahydride; In 1,4-dioxane; 1,2-dimethoxyethane; benzene;
DOI:10.1021/ja00202a058

Reference yield:

: 123074-23-7
1,1,1-Tris(carboxyethoxymethyl)ethane trimethyl ester

: 123074-28-2
1,13-Dimethyl-3,11,15,23,26,34-hexaoxa-6,20,29-trioxo-7,19,30-trisbenzyloxyazabicyclo<11,11,11>pentatriacontane

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / LiAlH₄

3: 1,2-dimethoxy-ethane

4: 30 percent / benzene

With lithium aluminium tetrahydride; In 1,2-dimethoxyethane; benzene;
DOI:10.1021/ja00202a058