2-methyl-1-butyl 3-[4-(3,4,5-triacetyloxybenzoyloxy)-3-methoxyphenyl]-2-propenoate

Base Information

Chemical Name:2-methyl-1-butyl 3-[4-(3,4,5-triacetyloxybenzoyloxy)-3-methoxyphenyl]-2-propenoate
CAS No.:515835-79-7
Molecular Formula:C₂₈H₃₀O₁₁
Molecular Weight:542.54
Hs Code.:

Synonyms:2-methyl-1-butyl 3-[4-(3,4,5-triacetyloxybenzoyloxy)-3-methoxyphenyl]-2-propenoate

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Chemical Property of 2-methyl-1-butyl 3-[4-(3,4,5-triacetyloxybenzoyloxy)-3-methoxyphenyl]-2-propenoate

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Technology Process of 2-methyl-1-butyl 3-[4-(3,4,5-triacetyloxybenzoyloxy)-3-methoxyphenyl]-2-propenoate

There total 3 articles about 2-methyl-1-butyl 3-[4-(3,4,5-triacetyloxybenzoyloxy)-3-methoxyphenyl]-2-propenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 70475-59-1
3,4,5-triacetoxybenzoyl chloride

: (E)-3-(4-Hydroxy-3-methoxy-phenyl)-acrylic acid 2-methyl-butyl ester

: 515835-79-7
2-methyl-1-butyl 3-[4-(3,4,5-triacetyloxybenzoyloxy)-3-methoxyphenyl]-2-propenoate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1016/S0968-0896(01)00361-3

Reference yield:

: 6635-24-1
3,4,5-triacetoxybenzoic acid

: 515835-79-7
2-methyl-1-butyl 3-[4-(3,4,5-triacetyloxybenzoyloxy)-3-methoxyphenyl]-2-propenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / SOCl₂ / CHCl₃

2: 67 percent / Et₃N / CH₂Cl₂ / 4 h / 20 °C

With thionyl chloride; triethylamine; In dichloromethane; chloroform;
DOI:10.1016/S0968-0896(01)00361-3

Reference yield:

: 149-91-7
3,4,5-trihydroxybenzoic acid

: 515835-79-7
2-methyl-1-butyl 3-[4-(3,4,5-triacetyloxybenzoyloxy)-3-methoxyphenyl]-2-propenoate

Guidance literature:: Multi-step reaction with 3 steps

1: aq. NaOH

2: 100 percent / SOCl₂ / CHCl₃

3: 67 percent / Et₃N / CH₂Cl₂ / 4 h / 20 °C

With sodium hydroxide; thionyl chloride; triethylamine; In dichloromethane; chloroform;
DOI:10.1016/S0968-0896(01)00361-3