Pd(dppe)(o-MeOC₆H₄)(I)

Base Information

Chemical Name:Pd(dppe)(o-MeOC₆H₄)(I)
CAS No.:586945-04-2
Molecular Formula:C₃₃H₃₁IOP₂Pd
Molecular Weight:738.881
Hs Code.:

Pd(dppe)(o-MeOC<sub>6</sub>H<sub>4</sub>)(I)

Synonyms:Pd(dppe)(o-MeOC₆H₄)(I)

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Chemical Property of Pd(dppe)(o-MeOC₆H₄)(I)

Chemical Property:

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Technology Process of Pd(dppe)(o-MeOC₆H₄)(I)

There total 2 articles about Pd(dppe)(o-MeOC₆H₄)(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 180891-47-8
trans-Pd(PPh₃)2(o-MeOC₆H₄)(I)

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 586945-04-2
Pd(dppe)(o-MeOC₆H₄)(I)

Guidance literature:: In toluene; under N2; at room temp.; soln. of dppe in toluene added to soln. of the Pd complex in toluene; suspn. stirred for 45 min; toluene removed in vacuo; petroleum ether added; soln. stirred for 12 h;solid collected on fine frit and dried; sample for anal. recrystd. from CHCl3/ether at -25 °C; elem. anal.;
DOI:10.1021/om030144x

Reference yield:

: 529-28-2
4-iodoanisol

: 586945-04-2
Pd(dppe)(o-MeOC₆H₄)(I)

Guidance literature:: Multi-step reaction with 2 steps

1: toluene

2: toluene

In toluene;
DOI:10.1021/om030144x

Reference yield:

: 586945-04-2
Pd(dppe)(o-MeOC₆H₄)(I)

: 501381-03-9,119186-75-3,136172-50-4
(+/-)-methylphenylphosphane borane

: 529-28-2
4-iodoanisol

: 31277-98-2
bis[1,2-bis(diphenylphosphino)ethane]palladium⁽⁰⁾

: 129212-59-5,97764-41-5,97858-63-4
(R(P))-(o-anisyl)(methyl)(phenyl)phosphine-P-borane

: 19998-21-1
[PdI₂(1,2-bis(diphenylphosphino)ethane)]

Guidance literature:: With NaOSiMe₃; In tetrahydrofuran; tetrahydrofuran-d8; under N2; at room temp.; PH(Me)(Ph)(BH3) and o-AnI added to soln. of Pd(dppe)(o-An)(I) in THF; NaOSiMe3 in THF added; soln. mixed; THF-d8 added;react. monitored by 31P NMR for 48 h; not isolated;
DOI:10.1021/om030144x