N,N-dimethyl-4-(1-(4-(methylsulfonyl)phenyl)-1H-tetrazol-5-yl)benzenamine

Base Information

Chemical Name:N,N-dimethyl-4-(1-(4-(methylsulfonyl)phenyl)-1H-tetrazol-5-yl)benzenamine
CAS No.:1369787-41-6
Molecular Formula:C₁₆H₁₇N₅O₂S
Molecular Weight:343.409
Hs Code.:

Synonyms:N,N-dimethyl-4-(1-(4-(methylsulfonyl)phenyl)-1H-tetrazol-5-yl)benzenamine

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Chemical Property of N,N-dimethyl-4-(1-(4-(methylsulfonyl)phenyl)-1H-tetrazol-5-yl)benzenamine

Chemical Property:

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Technology Process of N,N-dimethyl-4-(1-(4-(methylsulfonyl)phenyl)-1H-tetrazol-5-yl)benzenamine

There total 4 articles about N,N-dimethyl-4-(1-(4-(methylsulfonyl)phenyl)-1H-tetrazol-5-yl)benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1369787-33-6
C₁₆H₁₇N₅S

: 1369787-41-6
N,N-dimethyl-4-(1-(4-(methylsulfonyl)phenyl)-1H-tetrazol-5-yl)benzenamine

Guidance literature:: With oxone; at 20 ℃; for 3h;
DOI:10.1016/j.bmcl.2012.01.093

Reference yield:

: 87970-46-5
N-(4-dimethylaminobenzoyl)imidazole

: 1369787-41-6
N,N-dimethyl-4-(1-(4-(methylsulfonyl)phenyl)-1H-tetrazol-5-yl)benzenamine

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 90 °C / Inert atmosphere

2: sodium azide; tetrachlorosilane / acetonitrile / 24 h / 90 °C / Inert atmosphere

3: oxone / 3 h / 20 °C

With oxone; sodium azide; tetrachlorosilane; In tetrahydrofuran; acetonitrile;
DOI:10.1016/j.bmcl.2012.01.093

Reference yield:

: 1325466-60-1
4-(dimethylamino)-N-(4-(methylthio)phenyl)benzamide

: 1369787-41-6
N,N-dimethyl-4-(1-(4-(methylsulfonyl)phenyl)-1H-tetrazol-5-yl)benzenamine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide; tetrachlorosilane / acetonitrile / 24 h / 90 °C / Inert atmosphere

2: oxone / 3 h / 20 °C

With oxone; sodium azide; tetrachlorosilane; In acetonitrile;
DOI:10.1016/j.bmcl.2012.01.093