aci-nitromethyl-benzene

Base Information

• Chemical Name: aci-nitromethyl-benzene
• CAS No.: 622-43-5
• Molecular Formula: C₇H₇NO₂
• Molecular Weight: 137.138
• Mol file: 622-43-5.mol

Synonyms:aci-nitromethyl-benzene

Chemical Property of aci-nitromethyl-benzene

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of aci-nitromethyl-benzene

There total 5 articles about aci-nitromethyl-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-nitro-1-phenylmethane (622-42-4) → phenylnitromethane nitronic acid (622-43-5)

Guidance literature:

With morpholine; In water; at 20 ℃; Rate constant; Equilibrium constant; other reagents; var. solvents; pH = 8.89;

DOI:10.1021/jo00249a040

Reference yield:

phenylnitromethane carbanion (12413-18-2) → phenylnitromethane nitronic acid (622-43-5)

Guidance literature:

With acetic acid; In water; at 20 ℃; Rate constant; other reagents; var. solvents;

DOI:10.1021/jo00249a040

Reference yield:

iodomethylbenzene (620-05-3) → aci-nitromethyl-benzene (622-43-5)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether; AgNO₂ / 0 °C

2: man stellt das Natriumsalz des Phenylisonitromethans dar und zersetzt dieses durch starke Salzsaeure

With silver(I) nitrite; diethyl ether;

upstream raw materials:

1-nitro-1-phenylmethane

iodomethylbenzene

phenylnitromethane carbanion

Downstream raw materials:

1-nitro-1-phenylmethane

benzohydroximoyl chloride

Benzaldoxime

Benzohydroxamic acid