Technology Process of C29H44N4O8SSi
There total 8 articles about C29H44N4O8SSi which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C6H9N3SO2; C23H37NO7Si;
With
benzotriazol-1-ol; triethylamine;
In
dichloromethane;
at 0 ℃;
for 0.25h;
With
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane;
at 0 - 20 ℃;
DOI:10.1055/s-0032-1317810
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: trifluoroacetic acid; triethylsilane / dichloromethane / 1 h / 20 °C
2.1: benzotriazol-1-ol; triethylamine / dichloromethane / 0.25 h / 0 °C
2.2: 0 - 20 °C
With
triethylsilane; benzotriazol-1-ol; triethylamine; trifluoroacetic acid;
In
dichloromethane;
DOI:10.1055/s-0032-1317810
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 16.5 h / 0 - 20 °C
2.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C
2.2: 0.5 h / -78 °C
3.1: 1H-imidazole / N,N-dimethyl-formamide / 13 h / 0 - 20 °C
4.1: sodium periodate; ruthenium(IV) oxide / water; tetrachloromethane; acetonitrile / 13 h / 20 °C
5.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C
5.2: 0.5 h / -78 °C
6.1: zinc; potassium dihydrogenphosphate / tetrahydrofuran / 16 h / Sonication
7.1: benzotriazol-1-ol; triethylamine / dichloromethane / 0.25 h / 0 °C
7.2: 0 - 20 °C
With
1H-imidazole; ruthenium(IV) oxide; sodium periodate; potassium dihydrogenphosphate; di-isopropyl azodicarboxylate; sodium hydride; benzotriazol-1-ol; triethylamine; triphenylphosphine; zinc;
In
tetrahydrofuran; tetrachloromethane; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;
1.1: |Mitsunobu Displacement;
DOI:10.1055/s-0032-1317810
