C₃₃H₃₆O₄

Base Information

Chemical Name:C₃₃H₃₆O₄
CAS No.:1286188-95-1
Molecular Formula:C₃₃H₃₆O₄
Molecular Weight:496.646
Hs Code.:

C<sub>33</sub>H<sub>36</sub>O<sub>4</sub>

Synonyms:C₃₃H₃₆O₄

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Chemical Property of C₃₃H₃₆O₄

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Technology Process of C₃₃H₃₆O₄

There total 7 articles about C₃₃H₃₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1286188-94-0
C₃₃H₄₀O₄

: 1286188-95-1
C₃₃H₃₆O₄

Guidance literature:: With N-chloro-succinimide; 4-oxo-2,2,6,6-tetramethylpiperidin-oxyl; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; potassium carbonate; In dichloromethane; water; at 20 ℃; for 1.5h; pH=8.6; chemoselective reaction;
DOI:10.1002/chem.201002927

Reference yield:

: 1286188-92-8
C₄₁H₄₈O₃Si

: 1286188-95-1
C₃₃H₃₆O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium bis(2-methoxyethoxy)aluminium dihydride / dichloromethane; toluene / -20 - 20 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 8 h / 85 °C / Molecular sieve; Sealed tube

2.2: 1 h / 85 °C / Sealed tube

3.1: N-chloro-succinimide; 4-oxo-2,2,6,6-tetramethylpiperidin-oxyl; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; potassium carbonate / dichloromethane; water / 1.5 h / 20 °C / pH 8.6

With N-chloro-succinimide; 4-oxo-2,2,6,6-tetramethylpiperidin-oxyl; tetrabutyl ammonium fluoride; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; potassium carbonate; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; dichloromethane; water; toluene;
DOI:10.1002/chem.201002927

Reference yield:

: 1286188-93-9
C₄₁H₅₀O₃Si

: 1286188-95-1
C₃₃H₃₆O₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 8 h / 85 °C / Molecular sieve; Sealed tube

1.2: 1 h / 85 °C / Sealed tube

2.1: N-chloro-succinimide; 4-oxo-2,2,6,6-tetramethylpiperidin-oxyl; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; potassium carbonate / dichloromethane; water / 1.5 h / 20 °C / pH 8.6

With N-chloro-succinimide; 4-oxo-2,2,6,6-tetramethylpiperidin-oxyl; tetrabutyl ammonium fluoride; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; potassium carbonate; In tetrahydrofuran; dichloromethane; water;
DOI:10.1002/chem.201002927