1-benzyl-5-methyl-1H-[1,2,3]triazole-4-carboxylic acid 1-(2,3:4,5-di-O-isopropylidene)-β-D-fructopyranose ester

Base Information

• Chemical Name: 1-benzyl-5-methyl-1H-[1,2,3]triazole-4-carboxylic acid 1-(2,3:4,5-di-O-isopropylidene)-β-D-fructopyranose ester
• CAS No.: 1119518-76-1
• Molecular Formula: C₂₃H₂₉N₃O₇
• Molecular Weight: 459.499

Synonyms:1-benzyl-5-methyl-1H-[1,2,3]triazole-4-carboxylic acid 1-(2,3:4,5-di-O-isopropylidene)-β-D-fructopyranose ester

Chemical Property of 1-benzyl-5-methyl-1H-[1,2,3]triazole-4-carboxylic acid 1-(2,3:4,5-di-O-isopropylidene)-β-D-fructopyranose ester

Chemical Property:

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Technology Process of 1-benzyl-5-methyl-1H-[1,2,3]triazole-4-carboxylic acid 1-(2,3:4,5-di-O-isopropylidene)-β-D-fructopyranose ester

There total 1 articles about 1-benzyl-5-methyl-1H-[1,2,3]triazole-4-carboxylic acid 1-(2,3:4,5-di-O-isopropylidene)-β-D-fructopyranose ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

C23H31NO7 + Methanesulfonyl azide (624-90-8,1516-70-7) → 1-benzyl-5-methyl-1H-[1,2,3]triazole-4-carboxylic acid 1-(2,3:4,5-di-O-isopropylidene)-β-D-fructopyranose ester (1119518-76-1)

Guidance literature:

C₂₃H₃₁NO₇; With sodium hydride; In acetonitrile; at 20 ℃; Inert atmosphere;

Methanesulfonyl azide; In acetonitrile; at 20 ℃; for 48h;

DOI:10.1016/j.ejmech.2008.02.047

Reference yield:

1-benzyl-5-methyl-1H-[1,2,3]triazole-4-carboxylic acid 1-(2,3:4,5-di-O-isopropylidene)-β-D-fructopyranose ester (1119518-76-1) → 1-benzyl-5-methyl-1H-[1,2,3]triazole-4-carboxylic acid 1-β-D-fructopyranose ester (1119518-90-9)

Guidance literature:

With water; trifluoroacetic acid; for 48h;

DOI:10.1016/j.ejmech.2008.02.047

upstream raw materials:

Methanesulfonyl azide

Downstream raw materials:

1-benzyl-5-methyl-1H-[1,2,3]triazole-4-carboxylic acid 1-β-D-fructopyranose ester

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