5-(4,6-bis-methoxymethoxy-biphenyl-3-yl)-4-naphthalen-1-yl-4H-[1,2,4]triazole-3-thiol

Base Information

Chemical Name:5-(4,6-bis-methoxymethoxy-biphenyl-3-yl)-4-naphthalen-1-yl-4H-[1,2,4]triazole-3-thiol
CAS No.:959838-34-7
Molecular Formula:C₂₈H₂₅N₃O₄S
Molecular Weight:499.59
Hs Code.:

Synonyms:5-(4,6-bis-methoxymethoxy-biphenyl-3-yl)-4-naphthalen-1-yl-4H-[1,2,4]triazole-3-thiol

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Chemical Property of 5-(4,6-bis-methoxymethoxy-biphenyl-3-yl)-4-naphthalen-1-yl-4H-[1,2,4]triazole-3-thiol

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Technology Process of 5-(4,6-bis-methoxymethoxy-biphenyl-3-yl)-4-naphthalen-1-yl-4H-[1,2,4]triazole-3-thiol

There total 3 articles about 5-(4,6-bis-methoxymethoxy-biphenyl-3-yl)-4-naphthalen-1-yl-4H-[1,2,4]triazole-3-thiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 959838-33-6
C₂₈H₂₇N₃O₅S

: 959838-34-7
5-(4,6-bis-methoxymethoxy-biphenyl-3-yl)-4-naphthalen-1-yl-4H-[1,2,4]triazole-3-thiol

Guidance literature:: With sodium hydroxide; In water; at 110 ℃; for 2h;

Reference yield:

: 959838-31-4
methyl 5-bromo-2,4-bis(methoxymethoxy)benzoate

: 959838-34-7
5-(4,6-bis-methoxymethoxy-biphenyl-3-yl)-4-naphthalen-1-yl-4H-[1,2,4]triazole-3-thiol

Guidance literature:: Multi-step reaction with 4 steps

1: potassium phosphate / dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate / toluene / 24.17 h / 20 - 105 °C

2: hydrazine / 1,4-dioxane / 100 °C

3: ethanol / 0.5 h / 70 °C

4: sodium hydroxide / water / 2 h / 110 °C

With sodium hydroxide; potassium phosphate; hydrazine; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; In 1,4-dioxane; ethanol; water; toluene; 1: Suzuki Coupling;

Reference yield:

: 959838-32-5
4,6-bis-methoxymethoxy-biphenyl-3-carboxylic acid methyl ester

: 959838-34-7
5-(4,6-bis-methoxymethoxy-biphenyl-3-yl)-4-naphthalen-1-yl-4H-[1,2,4]triazole-3-thiol

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine / 1,4-dioxane / 100 °C

2: ethanol / 0.5 h / 70 °C

3: sodium hydroxide / water / 2 h / 110 °C

With sodium hydroxide; hydrazine; In 1,4-dioxane; ethanol; water;